1-溴-4-(苯氧基甲基)苯合成路线 (共 16 条)
反应条件
potassium carbonate in acetone 48 h; Heating;
参考文献
Oelschlaeger; Glassl; Seeling; Wange; Listing; Jung
Pharmazie, 2001 , vol. 56, # 8 p. 620 - 625
反应条件
1: PhBF3(-)K(+) With 4-(N,N-dimethlyamino)pyridine; copper diacetate; 4 A molecular sieve in dichloromethane T=20°C; 0.0833333 h; 2: 4-bromobenzyl-alcohol With oxygen in dichloromethane T=20°C; 24 h;
参考文献
Quach, Tan D.; Batey, Robert A.
Organic Letters, 2003 , vol. 5, # 8 p. 1381 - 1384
反应条件
potassium carbonate in ethanol T=78°C; 5 h;
参考文献
Bratulescu, George; Bigot, Yves L.E.; Delmas, Michel; Pogany, Iuliu
Revue Roumaine de Chimie, 1998 , vol. 43, # 4 p. 321 - 326
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2146,2148
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2146,2148
反应条件
ethenetetracarbonitrile in dichloromethane also reaction with DDQ; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 55, # 5 p. 1554 - 1559
反应条件
1: 1-bromo-4-(phenoxymethyl)benzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.0833333 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran T=-78 - 23°C; Inert atmosphere;
参考文献
Schmid, Kyle M.; Jensen, Lasse; Phillips, Scott T.
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4363 - 4374
反应条件
benzenethiol sodium salt in water; dimethyl sulfoxide T=60°C; 4 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 11 p. 1601 - 1607
反应条件
in water; dimethyl sulfoxide T=60°C; 1.08333 h; Irradiationother time; Product distribution;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 11 p. 1601 - 1607
反应条件
benzenethiol sodium salt in water; dimethyl sulfoxide T=60°C; 4 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dneprovskii; Tuchkin
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 11 p. 1601 - 1607