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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
甲基三苯基碘化膦
合成路线
（共 247 条）
2065-66-9
甲基三苯基碘化膦
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Arylation; 15 h; Heating;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
2065-66-9
甲基三苯基碘化膦
+
66-99-9
2-萘甲醛
→
反应条件
827-54-3
2-乙烯基萘
反应条件
1: triphenyl-methyl-phosphonium iodide With n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; Wittig Olefination; 2: β-naphthaldehyde in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Bosiak, Mariusz J.; Rakowiecki, Marcin; Orlowska, Katarzyna J.; Kedziera, Dariusz; Adams, Joerg
Dyes and Pigments, 2013 , vol. 99, # 3 p. 803 - 811
104-53-0
苯丙醛
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
768-56-9
4-苯基-1-丁烯
反应条件
1: triphenyl-methyl-phosphonium iodide With potassium tert-butylate in benzene Wittig Olefination; 1 h; Cooling with iceRefluxInert atmosphere; 2: 3-phenyl-propionaldehyde in benzene T=20°C; Wittig Olefination; Cooling with iceInert atmosphere;
参考文献
Maity, Soham; Manna, Srimanta; Rana, Sujoy; Naveen, Togati; Mallick, Arijit; Maiti, Debabrata
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3355 - 3358
2065-66-9
甲基三苯基碘化膦
+
185099-67-6
N-叔丁氧羰基-去甲托品酮
→
反应条件
273207-57-1
反应条件
potassium tert-butylate in tetrahydrofuran; ethyl acetate
参考文献
Pfizer Inc.
Patent: US6194438 B1, 2001 ;
2065-66-9
甲基三苯基碘化膦
+
1131-62-0
3,4-二甲氧基苯乙酮
→
反应条件
30405-75-5
反应条件
1: triphenyl-methyl-phosphonium iodide With n-butyllithium in tetrahydrofuran; hexane T=0°C; Wittig Olefination; 0.5 h; 2: 1-(3,4-dimethoxyphenyl)ethan-1-one in tetrahydrofuran; hexane T=20°C; Wittig Olefination; 24 h;
参考文献
Gong, Wanchun; Liu, Yun; Xue, Jijun; Xie, Zhixiang; Li, Ying
Chemistry Letters, 2012 , vol. 41, # 12 p. 1597 - 1599
2065-66-9
甲基三苯基碘化膦
+
529-34-0
1-四氢萘酮
→
反应条件
25108-63-8
反应条件
n-butyllithium in tetrahydrofuran; hexane Wittig reaction; Inert atmosphereCooling with ice;
参考文献
Larsen, Casey R.; Grotjahn, Douglas B.
Journal of the American Chemical Society, 2012 , vol. 134, # 25 p. 10357 - 10360
33603-90-6
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
24182-36-3
反应条件
1: triphenyl-methyl-phosphonium iodide With n-butyllithium in tetrahydrofuran; Petroleum ether T=-40°C; 0.833333 h; 2: α-bromocinnamaldehyde in tetrahydrofuran; Petroleum ether T=20°C; 1 h; Further stages.;
参考文献
Goumans, Theodorus P. M.; Van Alem, Kaj; Lodder, Gerrit
European Journal of Organic Chemistry, 2008 , # 3 p. 435 - 443
50-00-0
+
1517-82-4
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
反应条件
n-butyllithium 1) hexane, C6H6, rt, 1 h; 2) hexane, C6H6, 1 h; 3) hexane, C6H6, reflux, 10 h; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mikolajczyk, Marian; Perlikowska, Wieslawa; Omelanczuk, Jan; Cristau, Henri-Jean; Perraud-Darcy, Anne
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9716 - 9722
7022-45-9
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
30439-34-0
反应条件
1: triphenyl-methyl-phosphonium iodide With potassium tert-butylate in diethyl ether T=20°C; 0.166667 h; 2: (methylsulphanyl)-benzaldehyde in diethyl ether T=20°C; 2 h; Further stages.;
参考文献
LEMCOFF, N. Gabriel; BEN-ASULY, Amos
Patent: US2014/155511 A1, 2014 ;
Location in patent: Paragraph 0059 ;
112-31-2
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
821-95-4
+
791-28-6
反应条件
Carbowax 6000 (liquid); potassium carbonate T=150°C; P=15 Torr;
参考文献
Angeletti, Enrico; Tundo, Pietro; Venturello, Paolo
Journal of the Chemical Society, Chemical Communications, 1983 , # 6 p. 269 - 271
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