丙烷-1,3-二(磺酰氯)合成路线 （共 10 条）
反应条件
sodium hydroxide; benzene
参考文献
I.G. Farbenind.
Patent: DE740723 , 1941 ;
DRP/DRBP Org.Chem.
参考文献
Chemische Berichte, , vol. 91, p. 1512,1514
反应条件
dihydrogen peroxide; trichlorophosphate in water; acetonitrile
T=25°C;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Abbasi, Jamshid
Tetrahedron, 2012 , vol. 68, # 25 p. 5095 - 5101
反应条件
phosphorus pentachloride
T=20 - 110°C;
参考文献
BELLUS HEALTH (INTERNATIONAL) LIMITED; KONG, Xianqi; LEVENS, Nigel; BOUZIDE, Abderrahim; CIBLAT, Stephane; FRENETTE, Richard; RENAUD, Johanne
Patent: WO2011/17800 A1, 2011 ;
Location in patent: Page/Page column 63 ;
反应条件
water; chlorine
T=40°C;
参考文献
Asinger; Schmidt; Ebendener
Chemische Berichte, 1942 , vol. 75, p. 40
反应条件
(i) Na2SO3, (ii) PCl5; Multistep reaction;
参考文献
Johnston,T.P. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 399 - 402
反应条件
phosphorus pentachloride; BaCl2
T=105 - 110°C; 3 h; Yield given;
参考文献
Jueschke, Ralf; Velayutham, David; Sartoria, Peter
Journal of Fluorine Chemistry, 1997 , vol. 83, # 2 p. 145 - 149
反应条件
tetrachloromethane; sulfur dioxide; chlorine
Irradiation.mit UV-Licht;
参考文献
I.G.Farbenind.
Patent: DE717680 , 1938 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Asinger; Schmidt; Ebendener
Chemische Berichte, 1942 , vol. 75, p. 40
反应条件
Produkt5: Dichlorpropansulfochlorid;
参考文献
I.G.Farbenind.
Patent: DE717680 , 1938 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Horn
Patent: US2174492 , 1938 ;
Full Text Show Details
Asinger; Schmidt; Ebendener
Chemische Berichte, 1942 , vol. 75, p. 40
参考文献
Johnston,T.P. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 399 - 402
