hydrogen iodide; sodium thiosulfate in methanol; dichloromethane; water; acetic acid

hydrogenchloride; tin

1: ethanol; potassium hydroxide / 18 h / Reflux 2: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; methanol / 4560.31 Torr View Scheme

1.1: sulfuric acid / 6 h / Reflux 2.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 85 °C / Inert atmosphere 3.1: sodium hydroxide / 1,4-dioxane; methanol / 2.5 h / 85 °C 3.2: 0.17 h 4.1: diphenyl phosphoryl azide; triethylamine / tetrahydrofuran / 6 h / 80 °C 5.1: ethanol; potassium hydroxide / 18 h / Reflux 6.1: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; methanol / 4560.31 Torr View Scheme

1: diphenyl phosphoryl azide; triethylamine / tetrahydrofuran / 6 h / 80 °C 2: ethanol; potassium hydroxide / 18 h / Reflux 3: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; methanol / 4560.31 Torr View Scheme

1.1: sodium hydroxide / 1,4-dioxane; methanol / 2.5 h / 85 °C 1.2: 0.17 h 2.1: diphenyl phosphoryl azide; triethylamine / tetrahydrofuran / 6 h / 80 °C 3.1: ethanol; potassium hydroxide / 18 h / Reflux 4.1: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; methanol / 4560.31 Torr View Scheme

暂无反应条件数据

in ethyl acetate