2-甲氧基-吡啶 1-氧化物合成路线 （共 18 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
RESEARCH TRIANGLE INSTITUTE; CARROLL, Frank Ivy; ONDACHI, Pauline Wanjiku
Patent: WO2012/24615 A1, 2012 ;
Location in patent: Page/Page column 56 ;
WO 2012/024615 A1
反应条件
sodium methylate 1 h; Heating;
参考文献
Wolfe, Saul; Yang, Kiyull; Weinberg, Noham; Shi, Zheng; Hsieh, Yih-Huang; Sharma, Rajendra Dev; Ro, Stephen; Kim, Chan-Kyung
Chemistry - A European Journal, 1998 , vol. 4, # 5 p. 886 - 902
反应条件
1: 60 percent / MCPBA / CHCl3 / 24 h / 65 - 70 °C 2: 50 percent / NaOMe / 1 h / Heating View Scheme
参考文献
Wolfe, Saul; Yang, Kiyull; Weinberg, Noham; Shi, Zheng; Hsieh, Yih-Huang; Sharma, Rajendra Dev; Ro, Stephen; Kim, Chan-Kyung
Chemistry - A European Journal, 1998 , vol. 4, # 5 p. 886 - 902
参考文献
Cignitti, Maurizio; Soccorsi, Laura; Gatta, Franco; Cotta-Ramusino, Marina
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1985 , vol. 41, # 11 p. 1287 - 1294
参考文献
den Hertog; van Ammers
Recueil des Travaux Chimiques des Pays-Bas, 1955 , vol. 74, p. 1160,1164
反应条件
in methanol T=80.7°C; ΔE(excit.), log A; other temp.; Rate constantThermodynamic data;
参考文献
Cito, Antonia M.das Gracas Carvalho; Lopes, Jose Arimateia Dantas; Miller, Joseph; Moran, Paulo J. S.
Journal of Chemical Research, Miniprint, 1983 , # 7 p. 1586 - 1592
反应条件
1: 48 percent / HNO3; H2SO4 / 100 °C 2: 98 percent / Fe; AcOH / 100 °C 3: 43 percent / NaNO2; NaBr; CuSO4 / H2SO4 / 0 °C 4: 100 percent / PdCl2(dppf); KOAc / dimethylformamide / 80 °C View Scheme
参考文献
RESEARCH TRIANGLE INSTITUTE; CARROLL, Frank Ivy; ONDACHI, Pauline Wanjiku
Patent: WO2012/24615 A1, 2012 ;
WO 2012/024615 A1
反应条件
sulfuric acid; nitric acid T=100°C;
参考文献
RESEARCH TRIANGLE INSTITUTE; CARROLL, Frank Ivy; ONDACHI, Pauline Wanjiku
Patent: WO2012/24615 A1, 2012 ;
Location in patent: Page/Page column 56 ;
WO 2012/024615 A1
反应条件
sulfuric acid; nitric acid T=75°C; 1.5 h;
参考文献
Webber; Bleckman; Attard; Deal; Kathardekar; Welsh; Janson; Matthews; Smith; Freer; Jordan; Bacquet; Howland; Booth; Ward; Hermann; White; Morse; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 6 p. 733 - 746
反应条件
sulfuric acid; nitric acid
参考文献
Schnekenburger; Riedel
Archiv der Pharmazie, 1982 , vol. 315, # 10 p. 825 - 831
