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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
(S)-环氧苯乙烷
合成路线
（共 118 条）
292638-84-7
→
反应条件
60-12-8
苯乙醇
+
20780-54-5
(S)-环氧苯乙烷
反应条件
glycerol in bis(2-ethylhexyl)phthalate pH=7.2; aq. phosphate bufferMicrobiological reaction; enantioselective reaction;
参考文献
Green Chemistry, , vol. 14, # 3 p. 645 - 653
292638-84-7
→
反应条件
20780-53-4
(R)-环氧苯乙烷
+
50410-67-8
+
20780-54-5
(S)-环氧苯乙烷
反应条件
pyridine; Oxonereg;; water-d2; sodium hydrogencarbonate; (S)-(-)-2-(diphenylmethyl)pyrrolidine in acetonitrile-D3 T=20°C; 4 h; Product distribution / selectivity;
参考文献
The University of Sheffield
Patent: US2003/195366 A1, 2003 ;
Location in patent: Page/Page column 5 ;
532-27-4
2-氯苯乙酮
→
反应条件
93-56-1
苯基乙二醇
+
20780-54-5
(S)-环氧苯乙烷
+
70111-05-6
(S)-(+)-2-氯-1-苯乙醇
反应条件
1: With Lactobacillus brevis alcohol dehydrogenase; isopropyl alcohol T=30°C; 4 h; aq. bufferEnzymatic reaction; 2: With Mycobacterium sp. GP1 halohydrin dehalogenase HheB T=30°C; 20 h; aq. bufferEnzymatic reaction; optical yield given as percent eestereoselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 4 p. 483 - 488
96-09-3
氧化苯乙烯
+
536-74-3
苯乙炔
→
反应条件
20780-53-4
(R)-环氧苯乙烷
反应条件
1: (R)-phenylethylene oxide With sodium azide; Agrobacterium radiobacter halohydrin dehalogenase pH=7.5; aq. potassium phosphate bufferEnzymatic reaction; 2: phenylacetylene With CuSO4‵5H2O; sodium L-ascorbate; (±)-MonoPhos optical yield given as percent ee;
参考文献
Chemical Communications, , vol. 46, # 6 p. 898 - 900
1781-78-8
环辛炔
+
6388-74-5
(P-硝基苯基)环氧乙烷
→
反应条件
20780-53-4
(R)-环氧苯乙烷
反应条件
sodium azide; Agrobacterium radiobacter halohydrin dehalogenase pH=7.5; 48 h; aq. potassium phosphate bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Chemical Communications, , vol. 46, # 6 p. 898 - 900
292638-84-7
+
67-56-1
甲醇
→
反应条件
20780-54-5
(S)-环氧苯乙烷
+
101-48-4
1,1-二甲氧基-2-苯基乙烷
反应条件
iodosylbenzene; iron (III) perchlorate in water investigation of reaction in the presence of various Lewis acids and BLM (Bleomycin A2); Product distributionMechanism;
参考文献
Tetrahedron Letters, , vol. 26, # 39 p. 4699 - 4702
39201-98-4
→
反应条件
20780-54-5
(S)-环氧苯乙烷
反应条件
1: 80 percent / LiAlH4 / 6 h / Ambient temperature 2: 1.) trimethyloxonium fluoroborate, 2.) HONa solution / 1.) THF, room temperature, 2.) 1 h View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 4 p. 435 - 438
1098336-72-1
→
反应条件
20780-54-5
(S)-环氧苯乙烷
反应条件
1: With n-butyllithium 2: Acidic conditions;
参考文献
Tetrahedron, , vol. 65, # 1 p. 383 - 388
292638-84-7
→
反应条件
20780-53-4
(R)-环氧苯乙烷
+
16355-00-3
(R)-1-苯基-1,2-乙二醇
+
20780-54-5
(S)-环氧苯乙烷
+
122-78-1
苯乙醛
反应条件
peracetic acid; Jacobsen's (S,S)-(salen)Co(III) catalyst; water; acetic acid in toluene; acetonitrile optical yield given as percent eeenantioselective reaction;
参考文献
Green Chemistry, , vol. 12, # 5 p. 815 - 827
292638-84-7
+
50-99-7
葡萄糖
→
反应条件
60-12-8
苯乙醇
+
20780-54-5
(S)-环氧苯乙烷
+
64-19-7
醋酸
反应条件
octane; ammonia; water; thiamine chloride hydrochloride; magnesium sulfate in bis(2-ethylhexyl)phthalate pH=7.2; aq. phosphate bufferMicrobiological reaction; enantioselective reaction;
参考文献
Green Chemistry, , vol. 12, # 5 p. 815 - 827
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