2,3,4,6-四甲基吡啶合成路线 （共 11 条）
反应条件
1: With trifluorormethanesulfonic acid
T=50°C; diacetylation; 1 h;
2: With ammonium hydroxide
Title compound not separated from byproducts;
参考文献
Roussel, Christian; Rajoharison, Harivelo G.; Metzger, Jacques
Revue Roumaine de Chimie, 1991 , vol. 36, # 4-7 p. 613 - 618
反应条件
methanol; palladium on activated charcoal; Lindlar's catalyst
Hydrogenation;
参考文献
Tsuda et al.
Pharmaceutical Bulletin, 1953 , vol. 1, p. 122,125
反应条件
1: thionyl chloride
2: palladium/calcium carbonate; methanol / Hydrogenation
View Scheme
参考文献
Tsuda et al.
Pharmaceutical Bulletin, 1953 , vol. 1, p. 122,125
反应条件
perchloric acid
Erhitzen des Reaktionsprodukts mit wss. Essigsaeure und Ammoniumacetat;
参考文献
Praill; Whitear
Proceedings of the Chemical Society, London, 1959 , p. 312
Journal of the Chemical Society, 1961 , p. 3573,3578
反应条件
perchloric acid
Erhitzen des Reaktionsprodukts mit wss. Essigsaeure und Ammoniumacetat;
参考文献
Praill; Whitear
Proceedings of the Chemical Society, London, 1959 , p. 312
Journal of the Chemical Society, 1961 , p. 3573,3578
反应条件
ammonium hydroxide; Nafion-H
1.) CCl4, 2.5 h, reflux; 2.) 1 h, 20 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rajoharison, H. Gerard; Roussel, Christian; Metzger, Jacques
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2157 - 2173
反应条件
ammonium hydroxide; Nafion-H
1.) CCl4, 2.5 h, reflux; 2.) 1 h, 20 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rajoharison, H. Gerard; Roussel, Christian; Metzger, Jacques
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2157 - 2173
反应条件
ammonium hydroxide; Nafion-H
1.) CCl4, 2.5 h, reflux; 2.) 1 h, 20 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rajoharison, H. Gerard; Roussel, Christian; Metzger, Jacques
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2157 - 2173
反应条件
und Erhitzen des Reaktionsprodukts mit Ammoniumacetat in Essigsaeure;
参考文献
Praill; Whitear
Proceedings of the Chemical Society, London, 1959 , p. 312
Journal of the Chemical Society, 1961 , p. 3573,3578
反应条件
und Erhitzen des Reaktionsprodukts mit Ammoniumacetat in Essigsaeure auf Siedetemperatur;
参考文献
Praill; Whitear
Proceedings of the Chemical Society, London, 1959 , p. 312
Journal of the Chemical Society, 1961 , p. 3573,3578
