N,N-二甲基三甲基硅胺合成路线 （共 111 条）
参考文献
Wiberg,N.; Uhlenbrock,W.
Chemische Berichte, 1971 , vol. 104, p. 2643 - 2645
参考文献
Itoh,K. et al.
Organometallics in Chemical Synthesis, 1970 , vol. 1, p. 23 - 30
反应条件
in solid matrix
onto a frozen soln. of Me3SiNMe2 in SO2 in an NMR-tube AsF5 is condensed at -196°C, warming to room temp.; monitored by NMR-spectroscopy;
参考文献
Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
参考文献
Schmutzler, Reinhard; Stelzer, Othmar; Weferling, Norbert
Chemische Berichte, 1988 , vol. 121, p. 391 - 396
反应条件
T=85 - 95°C; 2 h; other temp. and time tested;
参考文献
Kozyukov, V. P.; Kozyukov, Vik. P.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1386 - 1394,1222 - 1229
反应条件
silicon tetrafluoride
T=150°C;
参考文献
Airey,W. et al.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1971 , vol. 27, p. 1505 - 1506
参考文献
Gmelin Handbook: B: B-Verb.4, 3.3, page 51 - 64
反应条件
in hexane
Addn. of Me3SiNMe2 (hexane) to a stirred soln. of BCl3 (hexane) at -78°C.;
参考文献
Li, Bei-Li; Neilson, Robert H.
Inorganic Chemistry, 1986 , vol. 25, p. 361 - 364
反应条件
methanol
T=20°C; 24 h;
参考文献
Voronkov, M. G.; Vvedenskii, V. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 6 p. 1428 - 1429,1266 - 1267
反应条件
sodium iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Arend, Michael; Risch, Nikolaus
Synlett, 1997 , vol. 1997, # 8 p. 974 - 976
