2-苯基-1,2-环氧丙烷合成路线 （共 116 条）
参考文献
Eliel; Freeman
Journal of the American Chemical Society, 1952 , vol. 74, p. 923,925
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in hexane; anhydrous butyl ether T=0 - 20°C; 14 h; Title compound not separated from byproducts.;
参考文献
Hodgson, David M.; Fleming, Matthew J.; Stanway, Steven J.
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4763 - 4773
反应条件
Amberlite IRA-400; borohydride form; copper(II) sulfate in methanol T=65°C; Reduction; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 70, # 5 p. 1101 - 1107
反应条件
1: NaN3 / dioxane; H2O / 23 h / Heating 2: 50 percent / nitrosonium tetrafluoroborate / acetonitrile / 0.08 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 9 p. 1704 - 1705
参考文献
Chemische Berichte, , vol. 60, p. 1062
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 59, p. 204
反应条件
(S)-6,6'-bis(2,4,6-triisopropylphenyl)-1,1'-spirobiindan-yl-7,7'-diylhydrogen-N-triflyl phosphoramide in tetrahydrofuran; dichloromethane T=-78°C; 4 h; Schlenk technique; Reagent/catalystSolventTime; enantioselective reaction;
参考文献
Zhuang, Minyang; Du, Haifeng
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1460 - 1462
反应条件
1.1: benzene / Heating 1.2: 50 percent / benzene / Heating 2.1: 73 percent / TMSOTf; (i-Pr)2NEt / CH2Cl2 / 6 h / 20 °C View Scheme
参考文献
Okuma, Kentaro; Hirose, Yoshitaka; Shioji, Kosei
Chemistry Letters, 2002 , # 4 p. 438 - 439
反应条件
water 1) Et2O, -78 deg C to 20 deg C, 18 h; Yield given. Multistep reaction;
参考文献
Kauffmann, Thomas; Neiteler, Christel; Robbe, Sonja
Chemische Berichte, 1992 , vol. 125, # 11 p. 2409 - 2418
反应条件
water 1) Et2O, -78 deg C to 20 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kauffmann, Thomas; Neiteler, Christel; Robbe, Sonja
Chemische Berichte, 1992 , vol. 125, # 11 p. 2409 - 2418
反应条件
water 1) Et2O, -78 deg C to 20 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kauffmann, Thomas; Neiteler, Christel; Robbe, Sonja
Chemische Berichte, 1992 , vol. 125, # 11 p. 2409 - 2418
