1-(4-硝基苯甲酰)哌啶合成路线 （共 29 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethanol
参考文献
IRM LLC
Patent: US2005/124637 A1, 2005 ;
Location in patent: Page/Page column 9 ;
US 20050124637 A1
反应条件
in dichloromethane
T=0 - 20°C; 0.166667 h;
参考文献
IRM LLC
Patent: US2005/124637 A1, 2005 ;
Location in patent: Page/Page column 9 ;
US 20050124637 A1
反应条件
PS-carbodiimide; MP-carbonate; benzotriazol-1-ol in N,N-dimethyl-formamide
4 h;
参考文献
Lannuzel, Marc; Lamothe, Marie; Perez, Michel
Tetrahedron Letters, 2001 , vol. 42, # 38 p. 6703 - 6705
反应条件
thionyl chloride; dihydrogen peroxide in ethanol
T=25°C; 0.0166667 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Farrokhi, Azita
Tetrahedron, 2009 , vol. 65, # 36 p. 7658 - 7661
反应条件
1: 1-(4-carboxyphenyl)-3-(4-nitrophenyl)-2-pyrazolin-5-one; amino polystyrene With dacarbazine; 4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide
24 h;
2: 4-nitro-benzoic acid With dacarbazine; 4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide
24 h;
3: piperidine in tetrahydrofuran; dichloromethane
T=20°C; 1 h;
参考文献
Byun, Jang-Woong; Lee, Dong-Hoon; Lee, Yoon-Sik
Tetrahedron Letters, 2003 , vol. 44, # 44 p. 8063 - 8067
反应条件
tert.-butylhydroperoxide; copper (II) acetate monohydrate
T=82°C; Minisci Aromatic Substitution; 0.833333 h; Inert atmosphere;
参考文献
Cadoni, Roberta; Porcheddu, Andrea; Giacomelli, Giampaolo; De Luca, Lidia
Organic Letters, 2012 , vol. 14, # 19 p. 5014 - 5017,4
Title/Abstract Full Text Show Details
Cadoni, Roberta; Porcheddu, Andrea; Giacomelli, Giampaolo; De Luca, Lidia
Organic Letters, 2012 , vol. 14, # 19 p. 5014 - 5017
反应条件
tert.-butylhydroperoxide in acetonitrile
T=80°C; 5 h;
参考文献
Thomson, Jaclyn A.; Schafer, Laurel L.
Dalton Transactions, 2012 , vol. 41, # 26 p. 7897 - 7904
反应条件
1: N-chloro-succinimide / acetonitrile / 3 h / 20 °C / |Inert atmosphere
2: copper (II) acetate monohydrate; tert.-butylhydroperoxide / 0.83 h / 82 °C / |Inert atmosphere
View Scheme
参考文献
Cadoni, Roberta; Porcheddu, Andrea; Giacomelli, Giampaolo; De Luca, Lidia
Organic Letters, 2012 , vol. 14, # 19 p. 5014 - 5017,4
Title/Abstract Full Text Show Details
Cadoni, Roberta; Porcheddu, Andrea; Giacomelli, Giampaolo; De Luca, Lidia
Organic Letters, 2012 , vol. 14, # 19 p. 5014 - 5017
反应条件
triethylamine; 2-hydroxy-2-methyl-propionitrile
T=25°C; 3 h;
参考文献
Raj, I. Victor Paul; Sudalai
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8303 - 8306
反应条件
1: C26H22O2P(1+)*I(1-) With zinc trifluoromethanesulfonate in acetonitrile
T=60°C; 0.5 h; Inert atmosphere;
2: piperidine in acetonitrile
T=60°C; 6 h; Inert atmosphere;
参考文献
Mamidi, Narsimha; Manna, Debasis
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2386 - 2396
