1-(4-硝基苯甲酰)哌啶合成路线 （共 29 条）
反应条件
in water; dimethyl sulfoxide; acetonitrile
T=25°C; Kinetics;
参考文献
Jeon, Seong Hoon; Kim, Hyun Soo; Han, Young Joon; Kim, Min-Young; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2014 , vol. 35, # 2 p. 471 - 476
反应条件
1: dichloromethane
2: acetonitrile / 25 °C
View Scheme
参考文献
Um, Ik-Hwan; Bae, Ae-Ri; Um, Tae-Il
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1206 - 1212
反应条件
1.1: iodine / acetonitrile / 0.17 h / |Inert atmosphere
2.1: zinc trifluoromethanesulfonate / acetonitrile / 0.5 h / 60 °C / |Inert atmosphere
2.2: 6 h / 60 °C / |Inert atmosphere
View Scheme
参考文献
Mamidi, Narsimha; Manna, Debasis
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2386 - 2396
反应条件
1: triethylamine / diethyl ether
2: acetonitrile / 25 °C
View Scheme
参考文献
Um, Ik-Hwan; Bae, Ae Ri
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7510 - 7515
反应条件
hydrogenchloride in dimethyl sulfoxide; acetonitrile
T=25°C; Substitution; Kinetics;
参考文献
Um, Ik-Hwan; Min, Ji-Sook; Ahn, Jung-Ae; Hahn, Hyun-Joo
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5659 - 5663
反应条件
potassium chloride in ethanol
T=25°C; pH=11.12; Kinetics; Further Variations:pH-valuesconcentrations;
参考文献
Castro, Enrique A.; Bessolo, Jorge; Aguayo, Raul; Santos, Jose G.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8157 - 8161
反应条件
phosphate buffer; potassium chloride in ethanol; water
T=25°C; pH=7.55; Kinetics; Further Variations:pH-values;
参考文献
Castro, Enrique A.; Aguayo, Raul; Bessolo, Jorge; Santos, Jose G.
Journal of Organic Chemistry, 2005 , vol. 70, # 19 p. 7788 - 7791
反应条件
in toluene
0.0333333 h; Ambient temperature;
参考文献
Hanefeld, Wolfgang; Bercin, Erdogan
Archiv der Pharmazie (Weinheim, Germany), 1984 , vol. 317, # 1 p. 74 - 79
反应条件
in water; dimethyl sulfoxide
T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Lee, Ji-Youn; Ko, Seung-Hak; Bae, Sun-Kun
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5800 - 5803
反应条件
in water; dimethyl sulfoxide
T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Lee, Ji-Youn; Ko, Seung-Hak; Bae, Sun-Kun
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5800 - 5803
