in diethyl ether
in N2 atm, a suspension of HgCl2 in Et2O was added over 0.2 h with stirring to a soln. of LiC6H4OCH3 in Et2O, stirred overnight, CHCl3 and H2O were added; sepd., aq. layer was extd. with CHCl3, combined organic layers were dried over Na2SO4, evapd., washed with Et2O; elem. anal.;
参考文献
Saunders, David R.; Stephenson, Martin; Mawby, Roger J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2473 - 2478
TMAP in N,N-dimethyl-formamide
electrolytic reduction at mercury pool cathode; various potentials (various coulometric n values); other unsymmetrically substituted diphenyliodonium bromides; Product distributionMechanism;
参考文献
Mubarak, Mohammad S.; Peters, Dennis G.
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 673 - 677
TMAP; mercury in N,N-dimethyl-formamide
electrolysis (-0.90 to -1.40 V); Product distribution;
参考文献
Mubarak, Mohammad S.; Karras, Louis L.; Murcia, Noel S.; Bart, John C.; Stemple, Joseph Z.; Peters, Dennis G.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1065 - 1070
