triphenyl phosphite; sodium hydride; [Ir(μ-Cl)(1,5-cyclooctadiene)]2 in tetrahydrofuran
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takeuchi, Ryo; Kashio, Mikihiro
Journal of the American Chemical Society, 1998 , vol. 120, # 34 p. 8647 - 8655
Tsukahara, Yuhko; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3013 - 3014
1: 4-methoxy-phenol With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
2: trans-cinnamyl acetate With tetrakis(triethylphosphite)nickel(O) in tetrahydrofuran; N,N-dimethyl-formamide
T=50°C; 20 h; Further stages.;
lithium chloride; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=100°C; 40 h; other alkalimetal halides, other solvent, other silylating agent; other allylic acetates; Product distribution;
