10-甲基-7(h)-苯并[c]咔唑合成路线 （共 9 条）
反应条件
hydrogenchloride in 1,4-dioxane; water 8 h; Inert atmosphereReflux;
参考文献
Lim, Byong-Yun; Choi, Min-Kyung; Cho, Cheon-Gyu
Tetrahedron Letters, 2011 , vol. 52, # 45 p. 6015 - 6017
反应条件
hydrogenchloride in ethanol 1 h; Heating;
参考文献
Lim, Young-Kwan; Jung, Jin-Woo; Lee, Haiwon; Cho, Cheon-Gyu
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5778 - 5781
反应条件
1: 83 percent / P(tBu)3; Cs2CO3 / Pd(OAc)2 / toluene / 1.5 h / Heating 2: 23 percent / aq. HCl / ethanol / 1 h / Heating View Scheme
参考文献
Lim, Young-Kwan; Jung, Jin-Woo; Lee, Haiwon; Cho, Cheon-Gyu
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5778 - 5781
反应条件
1: 66 percent / xantphos; Cs2CO3 / Pd2(dba)3 / toluene / 48 h / 80 °C 2: 83 percent / P(tBu)3; Cs2CO3 / Pd(OAc)2 / toluene / 1.5 h / Heating 3: 23 percent / aq. HCl / ethanol / 1 h / Heating View Scheme
参考文献
Lim, Young-Kwan; Jung, Jin-Woo; Lee, Haiwon; Cho, Cheon-Gyu
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5778 - 5781
反应条件
1: aqueous methanol 2: palladium/charcoal; xylene View Scheme
参考文献
Buu-Hoi et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1053,1078
反应条件
1: aqueous methanol 2: palladium/charcoal; xylene View Scheme
参考文献
Buu-Hoi et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1053,1078
反应条件
palladium on activated charcoal; xylene
参考文献
Campaigne et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 487
反应条件
sodium disulfite Behandeln des entstandenen Produkts mit heisser maessig konz.Salzsaeure oder mit Natronlauge;
参考文献
Bucherer; Seyde
Journal fuer Praktische Chemie (Leipzig), 1908 , vol. <2>77, # 406 p. 408,411
Full Text Show Details
Bucherer; Schmidt,M.
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 79, p. 412,415
参考文献
Buu-Hoi et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1053,1078
