1: oxyde de diphenylphosphinomethylephenylcetone With sodium methylate in tetrahydrofuran
T=20°C; 0.166667 h;
2: (E)-(3-chloro-1-propenyl)benzene With sodium iodide in tetrahydrofuran
T=20°C; 18 h; Further stages.;
参考文献
Fox, David J.; Pedersen, Daniel Sejer; Warren, Stuart
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 16 p. 3102 - 3107
potassium carbonate; (.eta.5-pentamethylcyclopentadienyl)(methyl diphenylphosphinite)bis(acetonitrile)ruthenium(II) PF6 in dichloromethane
T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Mbaye, Mbaye D.; Demerseman, Bernard; Renaud, Jean-Luc; Toupet, Loic; Bruneau, Christian
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 7 p. 835 - 841
1: dimethyl(phenyl)silyl chloride With lithium in tetrahydrofuran
T=0°C; 5 h; Inert atmosphere;
2: With zinc(II) chloride in tetrahydrofuran; diethyl ether
T=0°C;
3: (E)-(3-chloro-1-propenyl)benzene Further stages;
参考文献
Vyas, Devendra J.; Oestreich, Martin
Chemical Communications, 2010 , vol. 46, # 4 p. 568 - 570
