1-叔丁氧基-4-硝基苯合成路线 (共 23 条)
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Bialecki, Maciej
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4878 - 4888
反应条件
zinc T=25°C; Etherification; 1 h;
参考文献
Bandgar; Kasture
Journal of Chemical Research - Part S, 2000 , # 5 p. 252 - 253
反应条件
nickel 1,3-dibenzylimidazolidene in N,N-dimethyl-formamide T=100°C; 16 h; Product distribution / selectivity;
参考文献
AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH
Patent: WO2008/136770 A1, 2008 ;
Location in patent: Page/Page column 35-36 ;
反应条件
1: T=40°C; 0.333333 h; Inert atmosphereSonicationneat (no solvent); 2: With erbium trifluoromethanesulfonate T=20°C; 2.5 h; Inert atmosphereneat (no solvent);
参考文献
Procopio, Antonio; Costanzo, Paola; Curini, Massimo; Nardi, Monica; Oliverio, Manuela; Paonessa, Rosina
Synthesis, 2011 , # 1 p. 73 - 78
参考文献
Okamoto,K. et al.
Bulletin of the Chemical Society of Japan, 1964 , vol. 37, # 2 p. 276 - 282
反应条件
18-crown-6 ether in tetrahydrofuran T=20°C; 0.0833333 h; Title compound not separated from byproducts;
参考文献
Palani; Jayaprakash, Karamil; Hoz, Shmaryahu
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4388 - 4391
反应条件
in ammonia T=-70°C; 0.75 h;
参考文献
Kizner, T. A.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 991 - 997
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1089 - 1096
反应条件
in tetrahydrofuran T=30°C; electron-transfer reaction between tert-butoxide ion and nitrobenzene; reaction in the presence of molecular oxygen, concentration dependence, isotope effect, mechanism; Product distributionRate constant;
参考文献
Guthrie, Robert D.; Nutter, Dale E.
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7478 - 7482
反应条件
18-crown-6 ether in tert-butyl alcohol T=75°C; Rate constant;
参考文献
Prato, Maurizio; Quintily, Ugo; Salvagno, Susanna; Scorrano, Giangranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 413 - 416
反应条件
(i) NaH, (ii) /BRN= 606923/; Multistep reaction;
参考文献
Day,C.E. et al.
Journal of Medicinal Chemistry, 1975 , vol. 18, p. 1065 - 1070