N-(3-苯基苯基)乙酰胺合成路线 （共 19 条）
反应条件
1: potassium hydroxide / tetrahydrofuran / 20 °C
2: 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium phosphate / toluene / 24 h / 110 °C / |Schlenk technique
View Scheme
参考文献
Li, Xiao-Jian; Zhang, Jin-Ling; Geng, Yu; Jin, Zhong
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5078 - 5084
反应条件
1: triethylamine / dichloromethane / 6 h / 0 - 20 °C
2: palladium diacetate; tricyclopentyl-phosphine; potassium carbonate / toluene / 8 h / 95 °C / |Glovebox
3: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 6 h / 0 - 20 °C
View Scheme
参考文献
Hong, Wan Pyo; Iosub, Andrei V.; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 37 p. 13664 - 13667
反应条件
1: sodium acetate; hydroxylamine hydrochloride / methanol / 4 h / |Reflux
2: triethylamine / dichloromethane / 6 h / 0 - 20 °C
3: palladium diacetate; tricyclopentyl-phosphine; potassium carbonate / toluene / 8 h / 95 °C / |Glovebox
4: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 6 h / 0 - 20 °C
View Scheme
参考文献
Hong, Wan Pyo; Iosub, Andrei V.; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 37 p. 13664 - 13667
反应条件
1: tin (II)-chloride; aqueous-ethanolic hydrochloric acid
View Scheme
参考文献
Blakey; Scarborough
Journal of the Chemical Society, 1927 , p. 3006
反应条件
1: magnesium sulfate; NaOH-solution
2: tin (II)-chloride; aqueous-ethanolic hydrochloric acid
View Scheme
参考文献
Blakey; Scarborough
Journal of the Chemical Society, 1927 , p. 3006
反应条件
1: magnesium sulfate; NaOH-solution
2: tin (II)-chloride; aqueous-ethanolic hydrochloric acid
View Scheme
参考文献
Blakey; Scarborough
Journal of the Chemical Society, 1927 , p. 3006
反应条件
1: alcoholic sulfate solution; pentyl nitrite / Diazotization
2: alcohol; tin dichloride; hydrochloric acid
3: benzene
View Scheme
参考文献
Fichter; Sulzberger
Chemische Berichte, 1904 , vol. 37, p. 882
反应条件
1: alcoholic KOH-solution
2: alcoholic sulfate solution; pentyl nitrite / Diazotization
3: alcohol; tin dichloride; hydrochloric acid
4: benzene
View Scheme
参考文献
Fichter; Sulzberger
Chemische Berichte, 1904 , vol. 37, p. 882
参考文献
Blakey; Scarborough
Journal of the Chemical Society, 1927 , p. 3006
