三乙氧基(4-甲氧苯基)硅烷合成路线 (共 36 条)
反应条件
copper(l) iodide; cesium fluoride; N,N-dimethyl-2-(diphenylphosphino)benzeneaniline in N,N-dimethyl-formamide
T=120°C; Hiyama Coupling; 24 h; Inert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Vangala, Adarsh S.; Giri, Ramesh
Organic Letters, 2013 , vol. 15, # 20 p. 5378 - 5381
反应条件
sodium hydroxide; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane
T=80°C; 4 h;
参考文献
Murata; Shimazaki; Watanabe; Masuda
Synthesis, 2001 , # 15 p. 2231 - 2233
反应条件
copper(l) iodide; cesium fluoride in N,N-dimethyl-formamide
T=120°C; Hiyama Coupling; 12 h; Inert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Vangala, Adarsh S.; Giri, Ramesh
Organic Letters, 2013 , vol. 15, # 20 p. 5378 - 5381
反应条件
sodium hydroxide; [PdCl2(P(3,4-(18-crown-6)-phenyl)2(C6H5))2]
T=140°C; 1.5 h;
参考文献
Gordillo, Alvaro; De Jesus, Ernesto; Lopez-Mardomingo, Carmen
Organic Letters, 2006 , vol. 8, # 16 p. 3517 - 3520
反应条件
sodium hydroxide; tetrabutylammomium bromide; 4,4'-dichlorobenzophenone oxime-derived palladacycle
T=120°C; Hiyama coupling; P=7500.6 Torr; 0.166667 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 7-8 p. 945 - 952
反应条件
tetrabutyl ammonium fluoride; antimony trichloride; acetic acid; palladium diacetate in acetonitrile
T=60°C; 34 h;
参考文献
Denmark, Scott E.; Amishiro, Nobuyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6997 - 7003