苯甲醇-Alpha,Alpha-d2合成路线 （共 34 条）
反应条件
lithium aluminium deuteride in tetrahydrofuran
6 h; Heating;
参考文献
O'Hagan, David; Goss, Rebecca J. M.; Meddour, Abdelkrim; Courtieu, Jacques
Journal of the American Chemical Society, 2003 , vol. 125, # 2 p. 379 - 387
反应条件
lithium aluminium deuteride in tetrahydrofuran
T=0 - 20°C;
参考文献
Yuan, Hao; Yoo, Woo-Jin; Miyamura, Hiroyuki; Kobayashi, Shu
Journal of the American Chemical Society, 2012 , vol. 134, # 34 p. 13970 - 13973
反应条件
lithium aluminium deuteride in diethyl ether
T=0 - 20°C; 2 h;
参考文献
Bejot, Romain; Tisserand, Steve; Li, De Run; Falck; Mioskowski, Charles
Tetrahedron Letters, 2007 , vol. 48, # 22 p. 3855 - 3858
反应条件
lithium aluminium deuteride in tetrahydrofuran
T=0°C; 2 h;
参考文献
Chen, Ping-Shu; Chou, Chin-Hsing
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 5 p. 597 - 600
反应条件
water-d2; RuCl2(PPh3)2
T=150°C; P=7600 Torr; 0.5 h; microwave irradiation;
参考文献
Takahashi, Masaaki; Oshima, Koichiro; Matsubara, Seijiro
Chemistry Letters, 2005 , vol. 34, # 2 p. 192 - 193
反应条件
lithium aluminium deuteride in tetrahydrofuran; diethyl ether
T=20°C; 2 h;
参考文献
Bialecki, Jason; Ruzicka, Josef; Attygalle, Athula B.
Journal of Mass Spectrometry, 2006 , vol. 41, # 9 p. 1195 - 1204
反应条件
[Rh(C2H4)2Cl]2; tri-tert-butyl phosphine in 1,4-dioxane; acetone
T=80°C;
参考文献
Pucheault, Mathieu; Darses, Sylvain; Genet, Jean-Pierre
Journal of the American Chemical Society, 2004 , vol. 126, # 47 p. 15356 - 15357
反应条件
samarium diiodide; lithium amide; water-d2 in tetrahydrofuran
Ambient temperature;
参考文献
Kamochi, Yasuko; Kudo, Tadahiro
Chemistry Letters, 1991 , # 5 p. 893 - 896
反应条件
potassium hydroxide
T=0°C; unter Stickstoff;
参考文献
Hauser; Hamrick; Stewart
Journal of Organic Chemistry, 1956 , vol. 21, p. 260
反应条件
acetic acid; nitrosyl chloride in diethyl ether
1.) -75 deg C, 30 min, 2.) -75 deg C, 5 min; Further byproducts given;
参考文献
Bakke, Jan M.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 2 p. 127 - 129
