9-硼二环[3.3.1]壬烷 二聚物合成路线 （共 39 条）
反应条件
in toluene T=60°C; 1 h; Inert atmosphereSealed tube;
参考文献
Yoshida, Mika; Ohmiya, Hirohisa; Sawamura, Masaya
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 11896 - 11899
反应条件
water; dihydrogen peroxide
treatment with aq. H2O2;;
参考文献
Gmelin Handbook: B: B-Verb.14, 5.6, page 212 - 224
反应条件
in benzene-d6
in NMR tube, 15 min; not isolated, detected by NMR;
参考文献
Noeth, H.; Staudigl, R.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1981 , vol. 481, p. 41 - 50
反应条件
in benzene-d6
in NMR tube, 30 min; not isolated, detected by NMR;
参考文献
Noeth, H.; Staudigl, R.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1981 , vol. 481, p. 41 - 50
反应条件
in not given
in NMR tube; not isolated, detected by NMR;
参考文献
Noeth, H.; Staudigl, R.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1981 , vol. 481, p. 41 - 50
反应条件
1: n-heptane
2: not given
View Scheme
参考文献
Idelmann, Peter; Mueller, Gerhard; Scheidt, Walter R.; Schuessler, Wilhelm; Seevogel, Klaus; Koester, Roland
Angewandte Chemie, 1984 , vol. 96, p. 145 - 146
反应条件
1: n-heptane
2: not given
View Scheme
参考文献
Idelmann, Peter; Mueller, Gerhard; Scheidt, Walter R.; Schuessler, Wilhelm; Seevogel, Klaus; Koester, Roland
Angewandte Chemie, 1984 , vol. 96, p. 145 - 146
反应条件
in benzene
reacting educts by heating from 20°C to 80°C; pptd. by cooling; elem. anal.;
参考文献
Koester, Roland; Synoradzki, Ludwik
Chemische Berichte, 1984 , vol. 117, # 9 p. 2850 - 2862
反应条件
in chloroform
dropping soln. of borabicyclo deriv. into 98percent soln. of phosphoric acid at 20-70°C (2 h), reacting for 4.5 h; filtering, evapg. in vac., purifn. with sublimation of by-product; elem. anal.;
参考文献
Koester, Roland; Synoradzki, Ludwik
Chemische Berichte, 1984 , vol. 117, # 9 p. 2850 - 2862
