3-甲基-2-环己烯-1-醇合成路线 （共 78 条）
反应条件
monofluoromethane; trimethylamine
T=37.5°C; Irradiationvar. nucleophiles, var. pressure of reagents, other alcohol and cyclic dienes; Product distributionMechanism;
参考文献
Dezi, Emanuela; Lombardozzi, Antonietta; Renzi, Gabriele; Pizzabiocca, Adriano; Speranza, Maurizio
Chemistry--A European Journal, 1996 , vol. 2, # 3 p. 323 - 334
反应条件
cerium(III) chloride
0.5 h; Heatingother aliphatic alcohols (EtOH, n-PrOH, i-PrOH, t-BuOH); reaction of cyclic allylic acetates, cyclic allylic alcohols and oxime acetates with aliphatic alcohols in the presence of Ce(III) chloride; Product distribution;
参考文献
Uzarewicz; Dresler
Polish Journal of Chemistry, 1998 , vol. 72, # 8 p. 1921 - 1930
反应条件
monofluoromethane; trimethylamine
T=37.5°C; Irradiationvar. nucleophiles, var. pressure of reagents, other alcohol and cyclic dienes; Product distributionMechanism;
参考文献
Dezi, Emanuela; Lombardozzi, Antonietta; Renzi, Gabriele; Pizzabiocca, Adriano; Speranza, Maurizio
Chemistry--A European Journal, 1996 , vol. 2, # 3 p. 323 - 334
反应条件
pyridine
T=25°C; 12 h;
参考文献
Spahic, Bojana; Thu, Truong Thi My; Schlosser, Manfred
Helvetica Chimica Acta, 1980 , vol. 63, # 5 p. 1236 - 1241
反应条件
potassium fluoride on basic alumina in toluene
2 h;
参考文献
Yadav, Veejendra K; Ganesh Babu; Mittal, Manish
Tetrahedron, 2001 , vol. 57, # 32 p. 7047 - 7051
反应条件
propionic acid
T=140°C;
参考文献
Jones, Graham B.; Huber, Robert S.; Chau, Sotheary
Tetrahedron, 1993 , vol. 49, # 2 p. 369 - 380
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
0.5 h; Heating;
参考文献
Iranpoor; Mottaghinejad
Synthetic Communications, 1995 , vol. 25, # 15 p. 2253 - 2260
反应条件
sodium hydride in dimethyl sulfoxide
T=65°C; 14 h;
参考文献
Buechi, George; Vogel, Dennis E.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5406 - 5408
反应条件
2: m-CPBA / CH2Cl2 / 1 h / -30 - 0 °C
3: Et3N / CH2Cl2 / 1 h / -55 °C
4: NH3(l), Na / tetrahydrofuran
View Scheme
参考文献
Johnston; Morgan; Oehlschlager; Ramaswamy
Tetrahedron Asymmetry, 1991 , vol. 2, # 5 p. 377 - 380
反应条件
silica-supported monomeric vanadium-oxo species
T=0°C; 8 h;
参考文献
Mitsudome, Takato; Sueoka, Shoichiro; Ikeda, Satoshi; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
ChemCatChem, 2013 , vol. 5, # 10 p. 2879 - 2882
