2-三苯基膦乙烯基丙酸乙酯合成路线 (共 81 条)
反应条件
in toluene T=100°C; Wittig Olefination; 24 h; Overall yield = 70 percent; Overall yield = 4.11 g;
参考文献
Eske, Angelika; Goldfuss, Bernd; Griesbeck, Axel G.; De Kiff, Alan; Kleczka, Margarethe; Leven, Matthias; Neudoerfl, Joerg-M.; Vollmer, Moritz
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1818 - 1829
反应条件
in dichloromethane T=0 - 20°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 54, # 25 p. 3227 - 3229
反应条件
manganese(IV) oxide in dichloromethane T=20°C; Wittig olefination; 24 h;
参考文献
Tetrahedron, , vol. 63, # 42 p. 10528 - 10533
反应条件
in 1,2-dichloro-ethane
参考文献
Ykman,P. et al.
Tetrahedron, 1973 , vol. 29, p. 195 - 198
反应条件
Dehydrochlorination; Wittig reaction;
参考文献
Shen, Ruwei; Huang, Xian
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3961 - 3964
反应条件
manganese(IV) oxide in dichloromethane T=20°C; Wittig olefination; 24 h;
参考文献
Tetrahedron, , vol. 63, # 42 p. 10528 - 10533
反应条件
in dichloromethane T=50°C; 28 h;
参考文献
Volkonskii, A. Yu.; Mysov, E. I.; Rokhlin, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 6 p. 1246 - 1257
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 6 p. 1356 - 1367
反应条件
Jacobsen's Co(SALEN)2 silica in dichloromethane T=20°C; 144 h;
参考文献
Avery, Thomas D.; Taylor, Dennis K.; Tiekink, Edward R.T.
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5531 - 5546
反应条件
in dichloromethane T=25°C;
参考文献
Avery, Thomas D.
Chemical Communications, 1998 , # 3 p. 333 - 334
反应条件
in dichloromethane T=20°C; Isomerization; cyclopropanation; 168 h;
参考文献
Avery, Thomas D.; Taylor, Dennis K.; Tiekink, Edward R.T.
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5531 - 5546