2-三苯基膦乙烯基丙酸乙酯合成路线 （共 81 条）
反应条件
triethylamine in dichloromethane
T=20°C;
参考文献
Fu, Chunling; Ma, Shengming
European Journal of Organic Chemistry, 2005 , # 18 p. 3942 - 3945
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998
参考文献
Froyen,P.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1974 , vol. 28, p. 586 - 588
反应条件
Benzoesaeure in benzene
2 h; Heating;
参考文献
Spitzner, Dietrich; Swoboda, Harald
Tetrahedron Letters, 1986 , vol. 27, # 11 p. 1281 - 1284
反应条件
1: toluene / 22 h / 0 - 20 °C / |Inert atmosphere
2: toluene-4-sulfonic acid / methanol / 17 h / 20 °C / |Inert atmosphere
3: phosphorus tribromide / diethyl ether / 1 h / 0 - 45 °C / |Inert atmosphere
View Scheme
参考文献
Shiina, Isamu; Umezaki, Yuma; Ohashi, Yoshimi; Yamazaki, Yuta; Dan, Shingo; Yamori, Takao
Journal of Medicinal Chemistry, 2013 , vol. 56, # 1 p. 150 - 159
反应条件
triethylamine in dichloromethane
T=0 - 20°C; Wittig reaction; 24 h;
参考文献
Trost; Pinkerton; Seidel
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12466 - 12476
反应条件
triethylamine in dichloromethane
T=22°C; 0.833333 h;
参考文献
Jung, Michael E.; Nishimura, Nobuko
Organic Letters, 2001 , vol. 3, # 13 p. 2113 - 2115
反应条件
tributyl-amine; 2-chloro-1-methyl-pyridinium iodide in toluene
T=110°C; 3 h;
参考文献
Kohl-Mines, Elisabeth; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1985 , vol. 68, p. 2244 - 2248
反应条件
in chloroform-d1
0.0833333 h; or NEt3;
参考文献
Abell, Andrew D.; Morris, Kathryn B.; Litten, J. Christopher
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5217 - 5221
