2-三苯基膦乙烯基丙酸乙酯合成路线 （共 81 条）
反应条件
in benzene
T=7°C; 72 h; Title compound not separated from byproducts;
参考文献
Abell, Andrew D.; Morris, Kathryn B.; Litten, J. Christopher
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5217 - 5221
反应条件
triethylamine in dichloromethane
2 h; Inert atmosphere;
参考文献
Shi, Yili; Roth, Katrina E.; Ramgren, Stephen D.; Blum, Suzanne A.
Journal of the American Chemical Society, 2009 , vol. 131, # 50 p. 18022 - 18023
反应条件
triethylamine in dichloromethane
T=0 - 20°C; Wittig reaction; 24 h;
参考文献
Trost; Pinkerton; Seidel
Journal of the American Chemical Society, 2001 , vol. 123, # 50 p. 12466 - 12476
参考文献
Aksnes,G.; Froyen,P.
Acta Chemica Scandinavica (1947-1973), 1968 , vol. 22, p. 2347 - 2352
反应条件
in tetrahydrofuran
Heating;
参考文献
Shen, Ruwei; Huang, Xian
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3961 - 3964
反应条件
in toluene
T=100°C; Wittig Olefination; 24 h; Overall yield = 69 percent; Overall yield = 373 mg;
参考文献
Eske, Angelika; Goldfuss, Bernd; Griesbeck, Axel G.; De Kiff, Alan; Kleczka, Margarethe; Leven, Matthias; Neudoerfl, Joerg-M.; Vollmer, Moritz
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1818 - 1829
反应条件
in tetrahydrofuran
48 h; Heating;
参考文献
Dahmann, Georg; Hoffmann, Reinhard W.
Liebigs Annalen der Chemie, 1994 , # 8 p. 837 - 846
参考文献
Mali, R. S.; Yeola, Suresh N.; Kulkarni, B. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 4 p. 352 - 354
反应条件
in benzene
T=20°C; 10 h;
参考文献
Raghavan, Sadagopan; Sudheer Babu, Vaddela; Sridhar
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 557 - 565
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998
