4-甲基-4'-硝基联苯合成路线 （共 71 条）
反应条件
sodium hydroxide
T=5°C;
参考文献
France; Heilbron; Hey
Journal of the Chemical Society, 1939 , p. 1288,1291
Journal of the Chemical Society, 1940 , p. 369,370
反应条件
1: 1.) 1 M aq. HCl, NaNO2 / 1.) 0 deg C, 30 min, 2.) 0 deg C, 30 min
2: CF3COOH / 3 h / 65 - 70 °C
View Scheme
参考文献
Patrick, Timothy B.; Willaredt, Richard P.; DeGonia, David J.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2232 - 2235
反应条件
ammonium cerium(IV) nitrate in acetonitrile; benzene
24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1707 - 1714
反应条件
nitric acid; acetic acid
参考文献
Grieve; Hey
Journal of the Chemical Society, 1932 , p. 1888,1891
反应条件
hydrogenchloride
Diazotization.Behandlung der Diazoniumsalz-Loesung mit Toluol und wss. NaOH bei 5grad;
参考文献
France; Heilbron; Hey
Journal of the Chemical Society, 1939 , p. 1288,1291
Journal of the Chemical Society, 1940 , p. 369,370
反应条件
in dichloromethane
T=120 - 130°C; P=0.001 Torr; 2 h; Product distribution;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 457 - 464
反应条件
tert-Butyl thionitrate
1 h; Heating; Title compound not separated from byproducts;
参考文献
Oae, Shigeru; Shinhama, Koichi; Kim, Yong Hae
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 7 p. 2023 - 2026
反应条件
tert-Butyl thionitrate
2 h; Heating; Title compound not separated from byproducts;
参考文献
Oae, Shigeru; Shinhama, Koichi; Kim, Yong Hae
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 7 p. 2023 - 2026
参考文献
Robinson,G.E. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1971 , p. 1273 - 1282
参考文献
Grieve; Hey
Journal of the Chemical Society, 1932 , p. 1888,1891
