1-(4-硝基苯基)-N-[(4-硝基苯基)亚甲基氨基]甲亚胺合成路线 （共 23 条）
反应条件
selenium(IV) oxide in N,N-dimethyl-formamide T=100°C; 4 h;
参考文献
Dakova, B. Y.; Evers, M. J.; Christiaens, L. R.; Guillaume, M. R.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 3 p. 219 - 224
反应条件
PPh3 in acetic acid a stirred suspension of PdCl2 in anhyd. CH3COOH was treated with an excess of azine, refluxed for 45 min, cooled, treated with PPh3;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2441 - 2446
反应条件
in acetic acid a stirred suspension of PdCl2 in anhyd. CH3COOH was treated with an excess of azine, refluxed for 45 min, cooled, treated with PEt3;
参考文献
Granell, Jaime; Sales, Joaquim; Vilarrasa, Jaume; Declercq, Jean P.; Germain, Gabriel; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2441 - 2446
反应条件
1: 95 percent / selenium dioxide / dimethylformamide / 4 h / 100 °C 2: 1.) phenylhydrazine; 2.) selenium dioxide / 1.) DMF, 100 deg C, 1 h; 2.) 100 deg C, 1 h View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 3 p. 219 - 224
反应条件
dihydrogen peroxide T=80°C; 24 h;
参考文献
Polish Journal of Chemistry, , vol. 68, # 11 p. 2333 - 2342
反应条件
dihydrogen peroxide T=80°C; 24 h;
参考文献
Polish Journal of Chemistry, , vol. 68, # 11 p. 2333 - 2342
反应条件
1: 95 percent / selenium dioxide / dimethylformamide / 4 h / 100 °C 2: 1.) phenylhydrazine; 2.) selenium dioxide / 1.) DMF, 100 deg C, 1 h; 2.) 100 deg C, 1 h View Scheme
参考文献
Dakova, B. Y.; Evers, M. J.; Christiaens, L. R.; Guillaume, M. R.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 3 p. 219 - 224
反应条件
hydrazine hydrate; ethylenediamine; copper(l) chloride in ethanol
T=20°C; 24 h; 4;
参考文献
Nenajdenko, Valentine G.; Shastin, Alexey V.; Korotchenko, Vasily N.; Varseev, Georgy N.; Balenkova, Elisabeth S.
European Journal of Organic Chemistry, 2003 , # 2 p. 302 - 308
反应条件
Cu2Cl2; ammonium hydroxide in dimethyl sulfoxide
T=20°C; Oxidation; condensation; addition; elimination; 4 h;
参考文献
Korotchenko; Shastin; Nenaidenko; Balenkova
Russian Chemical Bulletin, 2003 , vol. 52, # 2 p. 492 - 497
反应条件
hydrazine hydrate in acetic acid
1 h; Ambient temperature;
参考文献
Mlochowski, J.; Giurg, M.
Polish Journal of Chemistry, 1994 , vol. 68, # 11 p. 2333 - 2342
