4-(4-氯苯氧基)苯酚合成路线 (共 16 条)
反应条件
1: With boron tribromide in dichloromethane T=-78 - 20°C; 2.08333 h; 2: With water in dichloromethane T=0°C; Product distribution / selectivity;
参考文献
DECODE CHEMISTRY, INC.
Patent: US2007/66820 A1, 2007 ;
Location in patent: Page/Page column 25; 27; 29 ;
US 20070066820 A1
反应条件
3-chloro-benzenecarboperoxoic acid Baeyer-Villiger oxidation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 10 p. 1801 - 1804
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 16 p. 2795 - 2798
反应条件
potassium hydroxide; hydrogen bromide; Copper(I)chloride in anhydrous xylene; acetic acid
参考文献
Hoechst Aktiengesellschaft
Patent: US4355189 A1, 1982 ;
反应条件
potassium tert-butylate in dimethyl sulfoxide T=170°C; 24 h;
参考文献
Marcune, Benjamin F.; Hillier, Michael C.; Marcoux, Jean-Francois; Humphrey, Guy R.
Tetrahedron Letters, 2005 , vol. 46, # 45 p. 7823 - 7826
反应条件
potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=170°C; 72 h;
参考文献
Marcune, Benjamin F.; Hillier, Michael C.; Marcoux, Jean-Francois; Humphrey, Guy R.
Tetrahedron Letters, 2005 , vol. 46, # 45 p. 7823 - 7826
反应条件
1: K2CO3 / N,N-dimethyl-acetamide / Heating 2: mCPBA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 10 p. 1801 - 1804
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 16 p. 2795 - 2798
反应条件
1: K2CO3 / N,N-dimethyl-acetamide / Heating 2: mCPBA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 10 p. 1801 - 1804
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 16 p. 2795 - 2798
反应条件
hydrogenchloride in methanol Heating; Yield given;
参考文献
Synthesis, , # 1 p. 63 - 68
反应条件
1: KOH 2: aq. HBr / acetic acid View Scheme
参考文献
FR2285861DE2543179 , ;
Chem.Abstr., , vol. 85, # 20843