2-甲氧基-2,4,6-环庚三烯-1-酮合成路线 （共 42 条）
反应条件
in chlorobenzene T=130°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 7 p. 2393 - 2399
反应条件
1: 24 percent / chlorobenzene / 12 h / 130 °C 2: 95 percent / chlorobenzene / 168 h / 120 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 7 p. 2393 - 2399
反应条件
1: ethanol / Heating 2: hot alkali View Scheme
参考文献
Nozoe, Tetsuo; Ishikawa, Sumio; Shindo, Kimio
Heterocycles, 1989 , vol. 28, # 2 p. 733 - 744
参考文献
Sci. Rep. Tohoku Univ., Ser. 1: Phys., Chem., Astron., , vol. # 37, p. 419,388,397
参考文献
Nozoe et al.
Tohoku Daigaku Hisui Yoeki Kagaku Kenkyusho Hokoku, 1957 , vol. 7, p. 13,19,21
Chem.Abstr., 1959 , p. 18885
反应条件
in chlorobenzene T=130°C; 20 h;
参考文献
Tian; Sugiyama; Mori; Takeshita
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 7 p. 2393 - 2399
反应条件
1.) 120 deg C, 3000 bar, 12 h; 2.) 120 deg C 7 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tian, Guan Rong; Sugiyama, Shigeru; Mori, Akira; Takeshita, Hitoshi
Chemistry Letters, 1987 , p. 1557 - 1560
反应条件
sodium hydride 1.) THF, 15 min, 2.) THF, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Irvine, Nicholas M.; Majewski, Marek
Organic Preparations and Procedures International, 1995 , vol. 27, # 5 p. 592 - 595
反应条件
1: Br2 / methanol 2: N2H4*H2O / diethyl ether 3: aq. HBr, CuSO4 View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1971 , vol. 44, # 8 p. 2218 - 2221
反应条件
ethanol; sodium ethanolate
参考文献
Nozoe et al.
Proceedings of the Japan Academy, 1953 , vol. 29, p. 452
Proceedings of the Japan Academy, 1954 , vol. 30, p. 483
