2,4-二乙酰基间苯三酚合成路线 (共 29 条)
反应条件
methanesulfonic acid; acetic acid T=80°C; 0.5 h; Neat (no solvent);
参考文献
Chauthe, Siddheshwar K.; Bharate, Sandip B.; Periyasamy, Giridharan; Khanna, Amit; Bhutani, Kamlesh K.; Mishra, Prabhu D.; Singh, Inder P.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 6 p. 2251 - 2256
反应条件
boron trifluoride diethyl etherate T=100°C; 2.5 h;
参考文献
Mudududdla, Ramesh; Jain, Shreyans K.; Bharate, Jaideep B.; Gupta, Ajai P.; Singh, Baldev; Vishwakarma, Ram A.; Bharate, Sandip B.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8821 - 8827
反应条件
boron trifluoride diethyl etherate; acetic acid 21 h; Heating;
参考文献
Nakagawa-Goto, Kyoko; Wu, Jiu-Hong; Bastow, Kenneth F.; Wu, Chin-Chung; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 6 p. 2325 - 2330
反应条件
zinc(II) chloride T=130°C;
参考文献
Chemische Berichte, , vol. 45, p. 418
Chemische Berichte, , vol. 42, p. 2738
反应条件
T=100°C; 2.5 h; Inert atmosphere;
参考文献
Furuta, Takumi; Nakayama, Miho; Suzuki, Hirotaka; Tajimi, Hiroko; Inai, Makoto; Nukaya, Haruo; Wakimoto, Toshiyuki; Kan, Toshiyuki
Organic Letters, 2009 , vol. 11, # 11 p. 2233 - 2236
反应条件
1: T=100°C; 3 h; 2: With potassium acetate in water T=20°C; 3 h;
参考文献
Vogel, Susanne; Barbic, Matej; Juergenliemk, Guido; Heilmann, Joerg
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 6 p. 2206 - 2213
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2708,2710
Journal of the Chemical Society, , p. 1241,1245
反应条件
zinc(II) chloride T=145 - 150°C; 0.25 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 823 - 826
反应条件
AlCl3, aluminium chloride in nitrobenzene T=50°C; Friedel Crafts acylation; 1 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 5 p. 2029 - 2036
反应条件
boron trifluoride diethyl etherate T=100°C; 2 h;
参考文献
Bioscience, biotechnology, and biochemistry, , vol. 56, # 11 p. 1769 - 1772