3,4-二甲氧基苯甲醛肟合成路线 (共 21 条)
反应条件
hydroxylamine hydrochloride; silica gel 0.0333333 h;
参考文献
Hajipour; Mohammadpoor-Baltork; Nikbaghat; Imanzadeh
Synthetic Communications, 1999 , vol. 29, # 10 p. 1697 - 1701
反应条件
hydroxylamine hydrochloride in methanol; diethyl ether T=20°C; 4 h;
参考文献
Synthetic Communications, , vol. 35, # 18 p. 2445 - 2451
反应条件
1: H2O2; Na2WO4 / methanol / 1 h / 20 °C 2: hydroxylamine hydrochloride / methanol; diethyl ether / 4 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 35, # 18 p. 2445 - 2451
反应条件
in acetonitrile byproducts: H2O, (Me2N)3P; addn. of Mo-complex to soln. of amine, treatment (35 min), pptn.; filtration off, washing (MeCN, Et2O), drying (vac.); elem. anal.;
参考文献
Journal of Molecular Catalysis, , vol. 83, p. 311 - 322
反应条件
1-benzyl-4-aza-1-azoniabiyclolt;2.2.2gt;octane peroxodisulfate in acetonitrile Oxidation; 0.25 h; Heating;
参考文献
Hajipour; Mallakpour
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 356, p. 371 - 387
反应条件
sodium hypochlorite in acetonitrile 0.5 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 4 p. 1091 - 1093
反应条件
sodium hypochlorite in acetonitrile 0.5 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 4 p. 1091 - 1093
反应条件
1: 78.5 percent / acetic anhydride / 0.5 h / Heating 2: 75 percent / hydrogen sulphide gas, triethylamine, pyridine / 6 h / Ambient temperature View Scheme
参考文献
Khadse, B. G.; Lokhande, S. R.; Bhamaria, R. P.; Prabhu, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 856 - 860
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether 14 h; Ambient temperature;
参考文献
Kano, Shinzo; Tanaka, Yasuyuki; Sugino, Eiichi; Hibino, Sstoshi
Synthesis, 1980 , # 9 p. 695 - 697
参考文献
Juliusberg
Chemische Berichte, 1907 , vol. 40, p. 120