反应条件
in tetrahydrofuran A soln. of 2-nitrosobiphenyl in THF under N2 is stirred at 25°C until it is light green (5 min), to soln. is added carbene complex in THF, the soln. is then heated under reflux for a period of 5 h.; cooling of resulting olive green soln. to 25°C, solvent removal, residue is dissolved in soln. of 19/1 hexane/ethyl acetate, purifn. by chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 368, p. 83 - 102
