2,3-二溴-3-苯丙酸甲酯合成路线 (共 13 条)
反应条件
hydrogenchloride; potassium hydroxide 1) MeOH, heating; Multistep reaction;
参考文献
Sharaf, Saber M.; El-Sadany, Samir K.; Hamed, Ezzat A.; Youssef, Abdel-Hamid A.
Canadian Journal of Chemistry, 1991 , vol. 69, # 9 p. 1445 - 1449
反应条件
bismuth(III) chloride; gallium in tetrahydrofuran T=20°C; 0.5 h; stereoselective reaction;
参考文献
Yoo, Byung Woo; Kim, Seo Hee; Park, Young Kwang
Synthetic Communications, 2012 , vol. 42, # 11 p. 1632 - 1636
反应条件
phosphorous acid trisdiethylamide in dichloromethane 24 h; Ambient temperature; Yields of byproduct given;
参考文献
Mizrakh, L. I.; Polonskaya, L. Yu.; Babushkina, T. A.; Ivanova, T. M.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 9 p. 2003 - 2008,1808 - 1811
反应条件
aluminum oxide; potassium fluoride in neat (no solvent) T=130°C; 0.5 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 39, # 23 p. 4035 - 4038
反应条件
triethylamine in N,N-dimethyl-formamide T=130°C; 0.75 h; microwave irradiation; Product distribution; Further Variations:ReagentsTemperaturesSolventsreaction time;
参考文献
Hamelin, Jack; Saoudi, Aicha; Benhaoua, Hadj
Synthesis, 2003 , # 14 p. 2185 - 2188
反应条件
iodine; magnesium in methanol 6 h; Ambient temperature;
参考文献
Khurana, Jitender M.; Gogia, Amita; Bankhwal, Ramesh K.
Synthetic Communications, 1997 , vol. 27, # 10 p. 1801 - 1809
反应条件
1: potassium hydroxide / ethanol / 6 h / Reflux 2: trifluoroacetic acid / 12 h / 60 °C View Scheme
参考文献
Sun, Jie; Ding, Wei Xian; Zhang, Ke Yun; Zou, Yong
Chinese Chemical Letters, 2011 , vol. 22, # 6 p. 667 - 670
反应条件
potassium hydroxide in ethanol 6 h; Reflux;
参考文献
Chinese Chemical Letters, , vol. 22, # 6 p. 667 - 670
反应条件
1: triethylamine 2: 87 percent / 0.5 h / 100 °C / high pressure 3: 83 percent / triethylamine / methanol / 2 h / Ambient temperature View Scheme
参考文献
Kashima, Choji; Tajima, Tadakuni; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 171 - 176
反应条件
tert-butylamine; bentonite
T=80°C; 0.5 h; Irradiation;
参考文献
Saoudi, Aicha; Hamelin, Jack; Benhaoua, Hadj
Journal of Chemical Research - Part S, 1996 , # 11 p. 492 - 493