(甲氧基羰基甲基)三苯基氯化鏻合成路线 （共 28 条）
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 40, # 7 p. 1683 - 1689
反应条件
1: (methoxycarbonylmethyl)triphenyl-phosphonium chloride With silver carbonate in acetonitrile
Wittig Olefination; 1 h;
2: furfural in acetonitrile
Wittig Olefination; Overall yield = 87 percent;
参考文献
Jedinak, Lukas; Rush, Latoya; Lee, Mijoon; Hesek, Dusan; Fisher, Jed F.; Boggess, Bill; Noll, Bruce C.; Mobashery, Shahriar
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12224 - 12228
反应条件
1: (methoxycarbonylmethyl)triphenyl-phosphonium chloride With silver carbonate in acetonitrile
Wittig Olefination; 1 h;
2: cyclohexanone in acetonitrile
Wittig Olefination;
参考文献
Jedinak, Lukas; Rush, Latoya; Lee, Mijoon; Hesek, Dusan; Fisher, Jed F.; Boggess, Bill; Noll, Bruce C.; Mobashery, Shahriar
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12224 - 12228
