5-溴甲基-1,2,3-三甲氧基苯合成路线 （共 19 条）
反应条件
phosphorus tribromide in benzene T=20°C;
参考文献
Parihar, Swati; Kumar, Amit; Chaturvedi, Amit K.; Sachan, Naresh Kumar; Luqman, Suaib; Changkija, Bendangla; Manohar, Murli; Prakash, Om; Chanda; Khan, Feroz; Chanotiya; Shanker, Karuna; Dwivedi, Anila; Konwar, Rituraj; Negi, Arvind S.
Journal of Steroid Biochemistry and Molecular Biology, 2013 , vol. 137, p. 332 - 344
反应条件
polymethylhydrosiloxane; bromo-dimethylsulfonium bromide in chloroform T=20°C; 5 h;
参考文献
Das, Biswanath; Srinivas, Yallamalla; Holla, Harish; Laxminarayana, Keetha; Narender, Ravirala
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6681 - 6683
反应条件
KBr-K222 complex; 1,2-dimethoxy-4-methylbenzene in tetrahydrofuran T=60°C; 0.0833333 h;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2005/23317 A1, 2005 ;
Location in patent: Page/Page column 17-18 ;
反应条件
bromine in tetrachloromethane Irradiationheating;
参考文献
Synthetic Communications, , vol. 35, # 6 p. 835 - 843
反应条件
pyridine; hydrogenchloride; sodium borohydride in tetrahydrofuran; water
反应条件
1: 70 percent / LAH / tetrahydrofuran 2: 80 percent / PBr3, triethylamine / CCl4 / 1) 1h, 0 degC 2) 3h, roomtemp. View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 3 p. 173 - 175
反应条件
1: 75 percent / dimethylsulfoxide / Ambient temperature 2: 92 percent / 3N KOH / Heating View Scheme
参考文献
Patra, Amarendra; Mukhopadhyay, Prabir K.; Ghosh, Gargi
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 173 - 175
反应条件
1.1: 73 percent / 2.17 h / 140 - 180 °C 2.1: 61 percent / NaH; 15-crown-5 / tetrahydrofuran 3.1: Na / tetrahydrofuran / 18 h / 20 °C 3.2: 69 percent / H2O / tetrahydrofuran / 0 °C View Scheme
参考文献
Azzena, Ugo; Dettori, Giovanna; Idini, Maria Vittoria; Pisano, Luisa; Sechi, Grazia
Tetrahedron, 2003 , vol. 59, # 40 p. 7961 - 7966
反应条件
sodium periodate in dichloromethane T=40 - 50°C; Ionic liquid;
参考文献
Hullio, Ahmed Ali; Mastoi; Khan, Khalid
Asian Journal of Chemistry, 2011 , vol. 23, # 12 p. 5411 - 5418
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane a.) -50 deg C, 30 min, b.) RT, 1.5 h;
参考文献
Mali; Jagtap
Synthetic Communications, 1991 , vol. 21, # 7 p. 841 - 848
