N-(2-氯乙基)甲烷磺酰胺合成路线 (共 7 条)
参考文献
Nippon Shokubai Co., Ltd.
Patent: US5210299 A1, 1993 ;
参考文献
Sumitomo Chemical Company, Limited
Patent: US3956385 A1, 1976 ;
反应条件
triethylamine in acetonitrile T=5 - 20°C;
参考文献
Kowalczyk, Bruce A.; Robinson III, James; Gardner, John O.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 116 - 121
参考文献
Gen.Aniline and Film Corp.
Patent: US2288178 , 1939 ;
反应条件
sodium iodide in butanone 2 h; RefluxInert atmosphereIndustrial scale;
参考文献
Kowalczyk, Bruce A.; Robinson III, James; Gardner, John O.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 116 - 121
反应条件
n-butyllithium; 1,10-phenanthroline; diisopropylamine in tetrahydrofuran; hexane T=-60 - 0°C; 2 h;
参考文献
Lee, Jaemoon; Zhong, Yong-Li; Reamer, Robert A.; Askin, David
Organic Letters, 2003 , vol. 5, # 22 p. 4175 - 4177
反应条件
anhydrous sodium hydrogen carbonate; sulfuric acid in methanol; water
参考文献
Sanko Chemical Company Ltd.
Patent: US4009205 A1, 1977 ;