4-(二甲基氨基甲酰)苯甲酸甲酯合成路线 (共 7 条)
反应条件
triethylamine; HATU in tetrahydrofuran T=20°C; 4 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY; CIANCI, Christopher, W.; GERRITZ, Samuel; LI, Guo; PEARCE, Bradley, C.; PENDRI, Annapurna; SHI, Shuhao; ZHAI, Weixu; ZHU, Shirong
Patent: WO2012/33736 A1, 2012 ;
Location in patent: Page/Page column 63 ;
反应条件
bis(tri-tert-butylphosphine)palladium(0) in toluene T=100°C; 10 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
Title/Abstract Full Text View citing articles Show Details
Sunada, Yusuke; Kawakami, Hiroko; Imaoka, Tsuyoshi; Motoyama, Yukihiro; Nagashima, Hideo
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9511 - 9514
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1770 - 1771
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
反应条件
in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Yamada, Shinji; Abe, Misato
Tetrahedron, 2010 , vol. 66, # 45 p. 8667 - 8671
反应条件
2-picoline; benzoylaminobenzene; sodium tetrahydroborate
参考文献
Kikugawa,Y.
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 5 p. 1059 - 1063