2-(2-羟基乙氧基)苯甲醛合成路线 (共 10 条)
反应条件
tetraethylammonium bromide in ethyl acetate
参考文献
Cedona Pharmaceuticals B.V.
Patent: US5378718 A1, 1995 ;
反应条件
sodium hydroxide in water T=98°C; 16 h;
参考文献
He, Jinmei; Zheng, Jiyue; Liu, Jian; She, Xuegong; Pan, Xinfu
Organic Letters, 2006 , vol. 8, # 20 p. 4637 - 4640
反应条件
sodium hydroxide in water 16 h; Reflux;
参考文献
Purushothaman; Prasanna; Niranjana; Raghunathan; Nagaraj; Rengasamy
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 24 p. 7288 - 7291
反应条件
manganese(IV) oxide in chloroform T=80°C; 20 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 20 p. 4552 - 4555
反应条件
in N,N-dimethyl-formamide Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, p. 3891 - 3896
反应条件
n-butyllithium 1.) THF, methylcyclohexane, -65 deg C to rt, 2.) THF, methylcyclohexane, rt, 2 h; Yield givenMultistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 64, # 15 p. 5589 - 5592
反应条件
4-methyl-3-(2,4,6-trimethylphenyl)thiazolium perchlorate; triethylamine; Azobenzene in tetrahydrofuran T=80°C; 20 h; Inert atmosphere;
参考文献
Rose, Christopher A.; Zeitler, Kirsten
Organic Letters, 2010 , vol. 12, # 20 p. 4552 - 4555
反应条件
3-benzyl-4,5-dimethylthiazol-3-ium bromide; triethylamine; Azobenzene in tetrahydrofuran T=80°C; 20 h; Inert atmosphere;
参考文献
Rose, Christopher A.; Zeitler, Kirsten
Organic Letters, 2010 , vol. 12, # 20 p. 4552 - 4555
反应条件
potassium tert-butylate in tert-butyl alcohol; benzene
72 h;
参考文献
Brokatzky-Geiger, Juergen; Eberbach, Wolfgang
Chemische Berichte, 1984 , vol. 117, # 6 p. 2157 - 2192
反应条件
triethylamine in diethyl ether
Ambient temperature;
参考文献
Baldwin, Jack E.; Crossley, Maxwell J.; Klose, Thomas; O'Rear, Edgar A.; Peters, Mary K.
Tetrahedron, 1982 , vol. 38, # 1 p. 27 - 40