1-环己基-2-甲氧基苯合成路线 (共 29 条)
反应条件
Me4-DACH; magnesium; cobalt(II) chloride in tetrahydrofuran
T=0°C; Inert atmosphere;
参考文献
Czaplik, Waldemar Maximilian; Mayer, Matthias; Jacobi Von Wangelin, Axel
Synlett, 2009 , # 18 p. 2931 - 2934
反应条件
tri-ruthenium(0)dodecacarbonyl; di-tert-butyl peroxide; 1,4-di(diphenylphosphino)-butane
T=135°C; P=760.051 Torr; 12 h; Under airDarkness; regioselective reaction;
参考文献
Guo, Xiangyu; Li, Chao-Jun
Organic Letters, 2011 , vol. 13, # 19 p. 4977 - 4979
反应条件
FeCl2(N(C2H5)2CH2CH2NC(CH3)CHC(CH3)O) in diethyl ether
T=20°C; 1 h; Inert atmosphere;
参考文献
Yamaguchi, Yoshitaka; Ando, Hiroaki; Nagaya, Makoto; Hinago, Hideto; Ito, Takashi; Asami, Masatoshi
Chemistry Letters, 2011 , vol. 40, # 9 p. 983 - 985
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts alkylation; 4 h;
参考文献
Singh, Ravi P; Kamble, Rajesh M; Chandra, Kusum L; Saravanan; Singh, Vinod K
Tetrahedron, 2001 , vol. 57, # 1 p. 241 - 247
反应条件
Ni(acac)2; (Z)-3,3-dimethyl-1,2-bis(diphenylphosphino)-1-butene in CPME
12 h; Inert atmosphereReflux;
参考文献
Kanemura, Shigenari; Kondoh, Azusa; Yorimitsu, Hideki; Oshima, Koichiro
Synthesis, 2008 , # 16 art. no. C02708SS, p. 2659 - 2664
反应条件
digallium tetrachloride in carbon disulfide
24 h; Heating; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
digallium tetrachloride in carbon disulfide
48 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
hydrogen; Pd and La-containing zeolite catalyst
T=150 - 170°C; P=11250.9 - 18751.5 Torr; other catalysts; hydrohenation of phenol and its ether om bifunctional zeolite catalysts; Product distribution;
参考文献
Marchenko, L. S.; Levin, D. Z.; Plakhotnik, V. A.; Mortikov, E. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 81 - 84
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 94 - 98
反应条件
scandium tris(trifluoromethanesulfonate) in tetrachloromethane
T=80°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kotsuki, Hiyoshizo; Oshisi, Takeshi; Inoue, Motoshi
Synlett, 1998 , # 3 p. 255 - 256
参考文献
Birch,A.J.; Nadamuni,G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 545 - 552