反应条件
1: 75.4 percent / Mg, cuprous chloride / diethyl ether; tetrahydrofuran / 20 °C 2: 70.5 percent / NaH / paraffin; tetrahydrofuran / 1.) room temperature, 30 min, 2.) reflux, 2 h 3: 30 percent / H2SO4 / acetic acid; acetic anhydride / 2 h / 110 °C 4: 60 percent / pyridinium chlorochromate, celite / benzene / 16 h / Heating 5: 86 percent / 20percent NaOH / methanol / 1 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 18, # 18 p. 2259 - 2266
