5-氯-3-苯基-1H-吲哚合成路线 (共 8 条)
反应条件
palladium diacetate; lithium hydroxide hydrate in water T=110°C; 24 h; Inert atmosphere;
参考文献
MERCK SHARP and DOHME CORP.; MCCOMAS, Casey Cameron; LIVERTON, Nigel J.; HABERMANN, Joerg; KOCH, Uwe; NARJES, Frank; LI, Peng; PENG, Xuanjia; SOLL, Richard; WU, Hao; PALANI, Anandan; DAI, Xing; LIU, Hong; HE, Shuwen; DANG, Qung
Patent: WO2013/34048 A1, 2013 ;
Location in patent: Page/Page column 56 ;
反应条件
carbon monoxide; 4 A molecular sieve; [(η5-C5Me5)Ru(CO)2]2 in 1,4-dioxane T=170°C; P=38787.1 Torr; 48 h;
参考文献
Penoni, Andrea; Nicholas, Kenneth M.
Chemical Communications, 2002 , # 5 p. 484 - 485
反应条件
CuCl2*2H2O; copper in 1,4-dioxane T=100°C; 5 h; Inert atmosphere; regioselective reaction;
参考文献
Murru, Siva; Gallo, August A.; Srivastava, Radhey S.
European Journal of Organic Chemistry, 2011 , # 11 p. 2035 - 2038
反应条件
palladium (II) trifluoroacetate; oxygen; bis[2-(diphenylphosphino)phenyl] ether in toluene T=140°C; 30 h; regioselective reaction;
参考文献
Chen, Shanping; Liao, Yunfeng; Zhao, Feng; Qi, Hongrui; Liu, Saiwen; Deng, Guo-Jun
Organic Letters, 2014 , vol. 16, # 6 p. 1618 - 1621
反应条件
1: benzene / Heating 2: H2 / 10percent Pd/C / benzene / 20 °C View Scheme
参考文献
Penoni, Andrea; Volkmann, Jerome; Nicholas, Kenneth M.
Organic Letters, 2002 , vol. 4, # 5 p. 699 - 701
反应条件
1,10-phenanthroline; palladium diacetate; trifluoroacetic acid in chlorobenzene T=100°C; 12 h;
参考文献
Chen, Yongxin; Guo, Shuaibo; Li, Kangning; Qu, Jinpeng; Yuan, Hua; Hua, Qiuru; Chen, Baohua
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 711 - 715
反应条件
1: benzene / Heating 2: H2 / 10percent Pd/C / benzene / 20 °C View Scheme
参考文献
Penoni, Andrea; Volkmann, Jerome; Nicholas, Kenneth M.
Organic Letters, 2002 , vol. 4, # 5 p. 699 - 701
反应条件
Fe pythalocyanine in toluene RefluxInert atmosphere; regioselective reaction;
参考文献
Lamar, Angus A.; Nicholas, Kenneth M.
Tetrahedron, 2009 , vol. 65, # 19 p. 3829 - 3833