N-(苯基亚甲基)-环己胺合成路线 （共 53 条）
反应条件
tert.-butylhydroperoxide; dirhodium (II,II) caprolactamate in acetonitrile
T=20°C; 16 h; Product distribution / selectivity;
参考文献
UNIVERSITY OF MARYLAND, COLLEGE PARK
Patent: US2009/93638 A1, 2009 ;
Location in patent: Page/Page column 24-25 ;
反应条件
palladium 10 on activated carbon in N-dodecane; N,N-dimethyl acetamide
T=120°C; 6 h; Inert atmosphere;
参考文献
Jin, Xukang; Liu, Yuxiao; Lu, Qiongqiong; Yang, Dejun; Sun, Jiangkai; Qin, Shuangshuang; Zhang, Jingwu; Shen, Jiaxuan; Chu, Changhu; Liu, Renhua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3776 - 3780
反应条件
sodium methylate; potassium iodide in methanol
T=15°C; Electrochemical reaction;
参考文献
Okimoto, Mitsuhiro; Takahashi, Yukio; Numata, Kaori; Sasaki, Gaku
Heterocycles, 2005 , vol. 65, # 2 p. 371 - 375
反应条件
palladium
T=120°C; 10 h;
参考文献
Murahashi; Yoshimura; Tsumiyama; Kojima
Journal of the American Chemical Society, 1983 , vol. 105, # 15 p. 5002 - 5011
反应条件
4 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal
T=120°C; P=46543.3 Torr; 24 h;
参考文献
Lin, Yong-Shou; Alper, Howard
Angewandte Chemie - International Edition, 2001 , vol. 40, # 4 p. 779 - 781
反应条件
4 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal
T=120°C; P=62057.8 Torr; 24 h;
参考文献
Lin, Yong-Shou; Alper, Howard
Angewandte Chemie - International Edition, 2001 , vol. 40, # 4 p. 779 - 781
反应条件
1: With 2-fluoro-pyridine; trifluoromethylsulfonic anhydride in dichloromethane
T=-78 - 0°C; Inert atmosphere;
2: With triethylsilane in dichloromethane
T=0 - 25°C; Inert atmosphere;
3: With sodium hydrogencarbonate in dichloromethane; water
chemoselective reaction;
参考文献
Pelletier, Guillaume; Bechara, William S.; Charette, Andre B.
Journal of the American Chemical Society, 2010 , vol. 132, # 37 p. 12817 - 12819
反应条件
in dichloromethane
T=20°C; 4 h; Inert atmosphereMolecular sieve;
参考文献
Diaba, Faiza; Montiel, Juan A.; Martinez-Laporta, Agustin; Bonjoch, Josep
Tetrahedron Letters, 2013 , vol. 54, # 21 p. 2619 - 2622
反应条件
sulfur in benzene
0.333333 h; Heating;
参考文献
Aly, Moustafa F.; Grigg, Ronald
Tetrahedron, 1988 , vol. 44, # 23 p. 7271 - 7282
反应条件
in chloroform-d1
2 h; Inert atmosphere;
参考文献
Bandar, Jeffrey S.; Coscia, Rockford W.; Lambert, Tristan H.
Tetrahedron, 2011 , vol. 67, # 24 p. 4364 - 4370
