2,3-环氧丙基-4-甲氧基苯基醚合成路线 (共 20 条)
反应条件
sodium hydroxide in water T=82 - 85°C; 3 h;
参考文献
Shapenova; Belyatskii; Panicheva
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 7 p. 1017 - 1020
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 20 h; Ambient temperature;
参考文献
Schvartzapel, Andrea J.; Zhong, Li; Docampo, Roberto; Rodriguez, Juan B.; Gros, Eduardo G.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 15 p. 2314 - 2322
反应条件
potassium carbonate in butanone T=80°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 11 p. 3399 - 3404
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 20 p. 6108 - 6115
反应条件
1: 1.) KOH / 1.) DMSO, 5 min, 2.) DMSO, RT, 3 h 2: 77 percent / 3-(chloroperoxy)benzoic acid / CH2Cl2 / 20 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 15 p. 2314 - 2322
反应条件
tetrabutylammomium bromide; potassium carbonate in acetonitrile 10 h; Reflux;
参考文献
Helvetica Chimica Acta, , vol. 95, # 3 p. 491 - 501
反应条件
morpholine-borane; boron trifluoride diethyl etherate in diethyl ether 2 h; Ambient temperature; Product distribution;
参考文献
Smith, William B.
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3219 - 3220
反应条件
1.1: NaH / dimethylformamide / 0.5 h / 20 °C 1.2: 90 percent / dimethylformamide / 4 h / 80 °C 2.1: 92 percent / pyridinium chloroformate; 4A molecular sieve / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Lee, Jeewoo; Kang, Ji-Hye; Lee, Sang-Yoon; Han, Kee-Chung; Torres, Christina M.; Bhattacharyya, Dipak K.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 20 p. 4129 - 4139
反应条件
1: With sodium hydride Heating; 2: With 4 A molecular sieve; pyridinium chlorochromate in dichloromethane Further stages.;
参考文献
Choi, Yongseok; Pu, Yongmei; Peach, Megan L.; Kang, Ji-Hye; Lewin, Nancy E.; Sigano, Dina M.; Garfield, Susan H.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 15 p. 3465 - 3481
反应条件
dimethyl sulfoxide; bismuth mandelate T=80°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 34, # 16 p. 2601 - 2604
反应条件
T=20°C; 2 h; Irradiation; Quantum yield;
参考文献
Timpe, H.-J.; Garcia, C.; Fedtke, M.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 4 p. 616 - 626