5,15-二苯基-21H,23H-卟吩合成路线 (共 16 条)
参考文献
Manka; Lawrence
Tetrahedron Letters, 1989 , vol. 30, # 52 p. 7341 - 7344
反应条件
NaAuCl4*2H2O; [bis(acetoxy)iodo]benzene in dichloromethane T=25°C;
参考文献
Journal of Organic Chemistry, , vol. 74, # 1 p. 206 - 211
反应条件
tris-(dibenzylideneacetone)dipalladium(0); diphenylphosphine oxide in tetrahydrofuran T=60°C; Kumada Cross-Coupling; 6 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 23 p. 10488 - 10497
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 2 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 2 h;
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 11 p. 3293 - 3304
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 5 h; 2: With chloranil in dichloromethane 7 h; Further stages.;
参考文献
Organic Letters, , vol. 4, # 25 p. 4377 - 4380
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 18 h; Inert atmosphereDarkness; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 1 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 21 p. 8005 - 8020
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 4.5 h; Inert atmosphereDarkness; 2: With pyridine in dichloromethane T=20°C; 17 h; Inert atmosphere; 3: in formic acid T=20°C; 4.25 h;
参考文献
Tetrahedron Letters, , vol. 52, # 25 p. 3175 - 3178
反应条件
1: With trifluoroacetic acid in dichloromethane 16 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 1 h;
参考文献
Chemistry - A European Journal, , vol. 11, # 11 p. 3427 - 3442
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 18 h; Inert atmosphereDarkness; 2: With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane Inert atmosphere;
参考文献
Beyzavi, M. Hassan; Lentz, Dieter; Reissig, Hans-Ulrich; Wiehe, Arno
European Journal of Organic Chemistry, 2013 , # 2 p. 269 - 282
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 18 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 1 h; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 23 p. 3833 - 3848