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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
右旋酮洛芬
合成路线
（共 39 条）
1276111-31-9
→
反应条件
22161-81-5
右旋酮洛芬
反应条件
1: (2R,5R)-2-tert-butyl-3-methyl-5-phenyl-4-imidazolidinone*TCA; sodium hydrogencarbonate; copper(I) bromide / diethyl ether; toluene / 3 h / 0 °C / Inert atmosphere 2: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / diethyl ether; water; toluene; acetonitrile / 3 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 12 p. 4260 - 4263
25116-37-4
(3-碘苯基)(苯基)甲酮
→
反应条件
22161-81-5
右旋酮洛芬
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane 1.2: 3 h / 0 - 20 °C 2.1: (2R,5R)-2-tert-butyl-3-methyl-5-phenyl-4-imidazolidinone*TCA; sodium hydrogencarbonate; copper(I) bromide / diethyl ether; toluene / 3 h / 0 °C / Inert atmosphere 3.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / diethyl ether; water; toluene; acetonitrile / 3 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 12 p. 4260 - 4263
2835-78-1
3-氨基苯基苯甲酮
→
反应条件
22161-81-5
右旋酮洛芬
反应条件
1.1: toluene-4-sulfonic acid / acetonitrile 1.2: 2.5 h / 0 - 20 °C 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane 2.2: 3 h / 0 - 20 °C 3.1: (2R,5R)-2-tert-butyl-3-methyl-5-phenyl-4-imidazolidinone*TCA; sodium hydrogencarbonate; copper(I) bromide / diethyl ether; toluene / 3 h / 0 °C / Inert atmosphere 4.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / diethyl ether; water; toluene; acetonitrile / 3 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 12 p. 4260 - 4263
22071-15-4
酮洛芬
+
85-61-0
辅酶 A
→
反应条件
430438-74-7
+
22161-81-5
右旋酮洛芬
反应条件
adenylate kinase; pyruvate kinase; Phosphoenolpyruvate; recombinant Luciola lateralis luciferase; adenosine 5'-triphosphoric acid; Reduced nicotinamide-adenine dinucleotide; magnesium chloride; lactate dehydrogenase T=27°C; pH=7; aq. potassium phosphate bufferEnzymatic reaction; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 69, # 3-4 p. 140 - 146
114315-58-1
→
反应条件
22161-81-5
右旋酮洛芬
+
122674-99-1
反应条件
phosphate buffer; C. cylindracea lipase; [14C]-Dextromethorphan T=24°C; 192 h; without amine, enetioselectivity of hydrolysis; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 17 p. 6836 - 6841
60658-04-0
酮洛芬乙酯
→
反应条件
22161-81-5
右旋酮洛芬
+
136656-96-7
反应条件
in water Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 49, # 37 p. 8433 - 8440
74614-67-8
→
反应条件
22161-81-5
右旋酮洛芬
+
56105-81-8
(2R)-2-(3-苯甲酰基苯基)丙酸
反应条件
(4R,5R)-DIOP; chloro(1,5-hexadiene)rhodium(I) dimer; hydrogen; triethylamine; benzene in ethanol P=53200 Torr; 20 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Gazzetta Chimica Italiana, , vol. 110, # 2/3 p. 123 - 128
22161-81-5
右旋酮洛芬
→
反应条件
66067-43-4
3-乙基苯甲酮
反应条件
in phosphate buffer T=25°C; pH=7.4; Photolysis; Quantum yieldKinetics; Further Variations:Reagents;
参考文献
Li, Ming-De; Du, Yong; Chuang, Yung Ping; Xue, Jiadan; Phillips, David Lee
Physical Chemistry Chemical Physics, 2010 , vol. 12, # 18 p. 4800 - 4808
22161-81-5
右旋酮洛芬
→
反应条件
反应条件
water in acetonitrile Irradiation; Mechanism;
参考文献
Li, Ming-De; Du, Yong; Chuang, Yung Ping; Xue, Jiadan; Phillips, David Lee
Physical Chemistry Chemical Physics, 2010 , vol. 12, # 18 p. 4800 - 4808
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