5,6,7,8-四氢-2-萘胺合成路线 （共 45 条）
参考文献
Schroeter
Justus Liebigs Annalen der Chemie, 1922 , vol. 426, p. 132
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 5 °C 1.2: 60 °C 2.1: 2,2'-azo-bisisobutyronitrile; N-bromosuccinmide / tetrachloromethane / 1 h / 80 °C / Inert atmosphere 3.1: tetreamethyl ammonium hydroxide / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere 3.2: 16 h / 20 °C / Inert atmosphere 4.1: 50 - 180 °C / 40 Torr View Scheme
参考文献
Ricoh Company, Ltd.; GOTO, Daisuke; YAMAMOTO, Satoshi; SAGISAKA, Toshiya; KATO, Takuji; OKADA, Takashi; SHINODA, Masato; MATSUMOTO, Shinji; MOHRI, Masataka; YUTANI, Keiichiro
Patent: WO2011/30918 A1, 2011 ;
反应条件
2: selenium / 350 °C View Scheme
参考文献
Buu-Hoi; Jacquignon
Journal of the Chemical Society, 1951 , p. 2964,2966
参考文献
Traut,M.; Hecker,E.
Justus Liebigs Annalen der Chemie, 1968 , vol. 715, p. 214 - 222
反应条件
1: benzene 2: NaNO2, HCO2H View Scheme
参考文献
Johnston; McCaleb; Opliger; Montgomery
Journal of medicinal chemistry, 1966 , vol. 9, # 6 p. 892 - 911
反应条件
sulfuric acid; sodium nitrite Diazotization;
参考文献
Bamberger; Kitschelt
Chemische Berichte, 1890 , vol. 23, p. 885
反应条件
hydrogenchloride; sodium nitrite Diazotization.Eintragen in eine aus Natriumcyanid,Kupfer(I)-chlorid und wss. Ammoniak hergestellte Loesung;
参考文献
Sergiewskaja; Nichamkina
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 940,943
Chem.Abstr., 1946 , p. 6453
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C View Scheme
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
反应条件
hydrogenchloride; sodium azide; sodium acetate; sodium nitrite 1.) water, 3-7 deg C, water, room temp., 15 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1933 - 1938
参考文献
Chemische Berichte, , vol. 23, p. 885
