3-亚甲基-2,6-庚烷二酮合成路线 （共 42 条）
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
octanol; 1,4-diaza-bicyclo[2.2.2]octane
T=20°C; Baylis-Hillman reaction; 12 h;
参考文献
Park, Kwang-Su; Kim, Jinyoung; Choo, Hyunah; Chong, Youhoon
Synlett, 2007 , # 3 p. 395 - 398
反应条件
1,4-diaza-bicyclo[2.2.2]octane
T=20°C; Baylis-Hillman reaction; 50 h; neat (no solvent);
参考文献
Saikia, Monmi; Sarma, Jadab C.
Canadian Journal of Chemistry, 2010 , vol. 88, # 12 p. 1271 - 1276
反应条件
1,4-diaza-bicyclo[2.2.2]octane in methanol
T=20°C; Baylis-Hillman reaction; 12 h;
参考文献
Park, Kwang-Su; Kim, Jinyoung; Choo, Hyunah; Chong, Youhoon
Synlett, 2007 , # 3 p. 395 - 398
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
216 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
[Rh(H)(PEt3)3] in isopropyl alcohol
T=40°C; 40 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Shibata, Masahiro
Journal of Organometallic Chemistry, 1989 , vol. 377, p. 347 - 356
反应条件
[Rh(H)(PEt3)3] in isopropyl alcohol
T=40°C; 40 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Shibata, Masahiro
Journal of Organometallic Chemistry, 1989 , vol. 377, p. 347 - 356
反应条件
1,4-diaza-bicyclo[2.2.2]octane in acetonitrile
T=50 - 60°C; Baylis-Hillman reaction; 6 h;
参考文献
Lee, Ka Young; Kim, Jeong Mi; Kim, Jae Nyoung
Synlett, 2003 , # 3 p. 357 - 360
反应条件
1,4-diaza-bicyclo[2.2.2]octane in methanol
T=20°C; Baylis-Hillman reaction; 12 h;
参考文献
Park, Kwang-Su; Kim, Jinyoung; Choo, Hyunah; Chong, Youhoon
Synlett, 2007 , # 3 p. 395 - 398
反应条件
octanol; 1,4-diaza-bicyclo[2.2.2]octane
T=20°C; Baylis-Hillman reaction; 12 h;
参考文献
Park, Kwang-Su; Kim, Jinyoung; Choo, Hyunah; Chong, Youhoon
Synlett, 2007 , # 3 p. 395 - 398
