3-亚甲基-2,6-庚烷二酮合成路线 （共 42 条）
反应条件
tris(N,N-dimethylaminomethyl)phosphine in tetrahydrofuran
T=20°C; 24 h;
参考文献
Tang, Xiaofang; Zhang, Bo; He, Zhengrong; Gao, Ruili; He, Zhengjie
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 11-12 p. 2007 - 2017
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=20°C; Baylis-Hillman reaction; 40 h;
参考文献
Shi, Min; Li, Chao-Qun; Jiang, Jian-Kang
Tetrahedron, 2003 , vol. 59, # 8 p. 1181 - 1189
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
192 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
85 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
80 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
[Rh(acac)2(CO)2]; P[2,4,6-(OMe)3C6H2]3 in benzene
T=80°C; 24 h;
参考文献
Lerum, Ronald V.; Russo, Christopher M.; Marquez, Jocellie E.; Chisholm, John D.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3485 - 3491
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
216 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
192 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
