3-亚甲基-2,6-庚烷二酮合成路线 （共 42 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
100 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=20°C;
参考文献
Liu, Xinyuan; Zhao, Jinwei; Jin, Guifang; Zhao, Gang; Zhu, Shizheng; Wang, Shaowu
Tetrahedron, 2005 , vol. 61, # 15 p. 3841 - 3851
反应条件
1,4-diaza-bicyclo[2.2.2]octane
T=20°C; Baylis-Hillman reaction; 3 h; neat (no solvent);
参考文献
Saikia, Monmi; Sarma, Jadab C.
Canadian Journal of Chemistry, 2010 , vol. 88, # 12 p. 1271 - 1276
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
360 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
[Rh(acac)2(CO)2]; tris(4-methoxyphenyl)-phosphine in benzene
T=80°C; 24 h;
参考文献
Lerum, Ronald V.; Russo, Christopher M.; Marquez, Jocellie E.; Chisholm, John D.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3485 - 3491
反应条件
isopropyl alcohol; dihydridotetrakis(triphenylphosphine)ruthenium(II)
T=40°C; 40 h;
参考文献
Matsuda, Isamu; Shibata, Masahiro; Sato, Susumu
Journal of Organometallic Chemistry, 1988 , vol. 340, p. C5 - C7
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
240 h; Ambient temperature;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
RhCl(PMe3)3
T=60°C; 5 h; sealed ampul; Yield given. Yields of byproduct given;
参考文献
Kovalev, I. P.; Kolmogorov, Yu. N.; Ignatenko, A. V.; Vinogradov, M. G.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 5.2 p. 995 - 999
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1098 - 1103
反应条件
1,4-diaza-bicyclo[2.2.2]octane in tetrahydrofuran
72 h; Ambient temperatureother aldehydes, var. reaction time; Mechanism;
参考文献
Basavaiah, Deevi; Gowriswari, Vellanki V. L.; Dharma Rao, Polisetti; Bharathi, Tirumala K.
Journal of Chemical Research, Miniprint, 1995 , # 7 p. 1656 - 1673
反应条件
1,4-diaza-bicyclo[2.2.2]octane in chloroform-d1
T=24.84°C; Baylis-Hillman reaction; 2.77778 h; Kinetics;
参考文献
Idahosa, Kenudi C.; Molefe, Duduzile M.; Pakade, Vusumzi E.; Brown, Michael E.; Kaye, Perry T.
South African Journal of Chemistry, 2011 , vol. 64, p. 144 - 150
