1: ascorbic acid powder With palladium on carbon; hydrogen in water T=50°C; P=2585.81 Torr; 24 h; 2: methyl propen-2-yl ether With toluene-4-sulfonic acid in N,N-dimethyl-formamide T=20°C; 24 h; Inert atmosphere; 3: With sodium periodate; sodium hydroxide in water T=7 - 10°C; Inert atmosphere;
参考文献
Izgu, Enver Cagri; Burns, Aaron C.; Hoye, Thomas R.
Organic Letters, 2011 , vol. 13, # 4 p. 703 - 705