2,3-二氯-5-硝基-1,4-萘醌合成路线 （共 16 条）
反应条件
hydrogenchloride; acetic acid; tin(ll) chloride Behandlung des Produkts mit Eisenchlorid in Wasser;
参考文献
Goerner, Helmut
Journal of Photochemistry and Photobiology A: Chemistry, 2011 , vol. 224, # 1 p. 135 - 140
反应条件
1: aniline With FDMP resin; sodium cyanoborohydride; acetic acid in N,N-dimethyl-formamide T=25°C; 16 h; 2: 2,3-dichloro-1,4-dihydro-1,4-dioxo-5-nitronaphthalene With 2,6-di-tert-butyl-pyridine in dichloromethane T=25°C; 2 h; 3: With trifluoroacetic acid in dichloromethane T=25°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Blackburn, Christopher
Tetrahedron Letters, 2005 , vol. 46, # 9 p. 1405 - 1409
反应条件
sulfuric acid; nitric acid in water
T=70 - 80°C; 2.5 h;
参考文献
Sturgess, Michael Alan; Yang, Ke
Patent: US2003/232801 A1, 2003 ;
Location in patent: Page 24 ;
反应条件
sulfuric acid; nitric acid
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
Full Text Show Details
I. G. Farbenind.
Patent: DE468507 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 520
反应条件
iodine; chlorine in acetic acid
Heating;
参考文献
Jones, Gordon H.; Venuti, Michael C.; Young, John M.; Murthy, D.V. Krishna; Loe, Brad E.; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 8 p. 1504 - 1511
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
反应条件
1: glacial acetic acid; concentrated hydrochloric acid / bei der Chlorierung
2: NaHSO3; acetic acid / 80 °C
3: glacial acetic acid; nitric acid
4: concentrated sulfuric acid
View Scheme
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
反应条件
1: glacial acetic acid; nitric acid
2: concentrated sulfuric acid
View Scheme
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
反应条件
1: NaHSO3; acetic acid / 80 °C
2: glacial acetic acid; nitric acid
3: concentrated sulfuric acid
View Scheme
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
参考文献
Fries; Pense; Peeters
Chemische Berichte, 1928 , vol. 61, p. 1399
